Extraction method of Flos chrysanthemi indici volatile oil

An extraction method, the technology of wild chrysanthemum, is applied in the direction of essential oils/spices, fat production, etc., which can solve the problems of long extraction time, low extraction rate, organic solvent residue, etc., and achieve the effect of improving crushing efficiency and increasing benefits

Inactive Publication Date: 2016-07-27
CHONGQING UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] For the above-mentioned deficiencies existing in the prior art, the technical problem to be solved in the present invention is: for the extraction method of the volatile oil of the wild chrysanthemum in the prior art, there are organic solvent residues, easy introduction of impurities, low extrac...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] (1) Accurately weigh the dried wild chrysanthemum flowers with an analytical balance, first remove the receptacle, sepals and flower stalks of the dried wild chrysanthemums, and crush the petals to a powder with a particle size of 80 mesh to obtain dried wild chrysanthemum powder;

[0019] (2) Freeze and thaw the wild chrysanthemum dried flower powder obtained in step 1) repeatedly for 2-3 times (the first freeze-thaw process is to freeze at -4°C for 10 minutes and thaw at room temperature for 20 minutes), and then put it into a 500mL three-necked round-bottomed distillation flask , add deionized water with 8 times the mass of dried chrysanthemum flower powder, add 5g of artificial zeolite, and soak at 60°C for 2h;

[0020] (3) Add an appropriate amount of small glass beads to the sample prepared in step 2), put it into an ultrasonic cleaner for ultrasonic treatment, ultrasonic power: 200W, ultrasonic time: 30min, temperature 60°C;

[0021] (4) Using a reflux distillati...

Embodiment 2

[0026] (1) Accurately weigh the dried wild chrysanthemum flowers with an analytical balance, first remove the receptacles, sepals and flower stalks of the dried wild chrysanthemums, and crush the petals to a powder with a particle size of 90 mesh to obtain dried wild chrysanthemum powders;

[0027] (2) Freeze and thaw the wild chrysanthemum dried flower powder obtained in step 1) repeatedly for 2-3 times (the first freeze-thaw process is to freeze at -4°C for 10 minutes and thaw at room temperature for 20 minutes), and then put it into a 500mL three-necked round-bottomed distillation flask , add deionized water 10 times the mass of dried chrysanthemum flower powder, add 5g of artificial zeolite, and soak at 70°C for 1.5h;

[0028] (3) Add an appropriate amount of small glass beads to the sample prepared in step 2), put it into an ultrasonic cleaner for ultrasonic treatment, ultrasonic power: 200W, ultrasonic time: 40min, temperature 60°C;

[0029] (4) Using a reflux distillati...

Embodiment 3

[0034] (1) Accurately weigh the dried wild chrysanthemum flowers with an analytical balance, first remove the receptacle, sepals and flower stalks of the dried wild chrysanthemums, and crush the petals to a powder with a particle size of 100 mesh to obtain dried wild chrysanthemum flowers powder;

[0035](2) Freeze and thaw the wild chrysanthemum dried flower powder obtained in step 1) repeatedly for 2-3 times (the first freeze-thaw process is to freeze at -4°C for 10 minutes and thaw at room temperature for 20 minutes), and then put it into a 500mL three-necked round-bottomed distillation flask , add deionized water with 12 times the mass of dried chrysanthemum flower powder, add 5g of artificial zeolite, and soak at 60°C for 2h;

[0036] (3) Add an appropriate amount of small glass beads to the sample prepared in step 2), put it into an ultrasonic cleaner for ultrasonic treatment, ultrasonic power: 500W, ultrasonic time: 60min, temperature 60°C;

[0037] (4) Using a reflux d...

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Abstract

The invention provides an extraction method of Flos chrysanthemi indici volatile oil.The extraction method includes: removing receptacles, sepals and flower stalks of dry Flos chrysanthemi indici; smashing petals of the dry Flos chrysanthemi indici into Flos chrysanthemi indici powder, and repeatedly freezing and thawing for 2-3 times; adding into water of 60-70 DEG C for soaking for 1-2 h, and ultrasonically treating the Flos chrysanthemi indici powder after being soaked and extract; performing distillation extraction on the Flos chrysanthemi indici powder after being ultrasonically treated and the extract at 100-120 DEG C for 3-5 h, and collecting upper-layer oily substance in distillation condensate to obtain Flos chrysanthemi indici volatile oil crude extract; using macroporous resin to adsorb and desorb the Flos chrysanthemi indici volatile oil crude extract to obtain pure Flos chrysanthemi indici volatile oil.No additive or organic solvent is used in the method, so that original fragrance of volatile oil is retained; no organic solvent is left in the Flos chrysanthemi indici volatile oil, so that the extraction method is safer and pollution-free.The extraction method has the advantages that extraction rate is up to 7.5%, extraction time is short, and extracted volatile oil is higher in purity.

Description

technical field [0001] The invention belongs to the technical field of chemical extraction, and in particular relates to a method for extracting volatile oil from wild chrysanthemum flowers. Background technique [0002] Wild chrysanthemum is the dry flower head of Chrysanthemumindi-cum Lamb (Chrysanthemumindi-cum Lamb), also known as malaria grass, bitter barley, mountain chrysanthemum, etc., which is a perennial herb of Compositae. It has the functions of improving eyesight, clearing heat and detoxifying, stopping bleeding and reducing swelling, and has high medicinal value. The main components of wild chrysanthemum volatile oil (essential oil) are monoterpenes, sesquiterpenes and their oxygen-containing derivatives and aliphatic compounds. and insect repellent, and the unique fragrance of volatile oil is widely favored by the general public, and can be used in industries such as perfume and cosmetics. Therefore, chrysanthemum volatile oil has very broad development prosp...

Claims

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Application Information

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IPC IPC(8): C11B9/02
CPCC11B9/022
Inventor 侯长军陈飞霍丹群杨眉
Owner CHONGQING UNIV
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