Active energy ray curable resin composition and optical mirror for automobile headlamp
A curable resin and active energy ray technology, applied in the direction of headlights, synthetic resin layered products, lighting devices, etc., can solve the problems of reduced adhesion of the cured film, hinder deep curing of the coating film, etc., and achieve hardness and weather resistance excellent effect
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[0101] Hereafter, although an Example and a comparative example are given and this invention is demonstrated in more detail, this invention is not limited to the following example unless the summary is exceeded. Also "parts" means "parts by mass".
Synthetic example 1
[0102] Synthesis of urethane acrylate mixture UA-1 (component (B))
[0103] In a flask equipped with a dropping funnel, a reflux condenser, a stirring blade, and a temperature sensor, simultaneously add dicyclohexylmethane-4,4-diisocyanate (trade name: Desmodur W, Sumika Bayer ammonia) as a raw material for (b1) 1310 g (5 moles) of Ester Co., Ltd.) and 0.5 g of di-n-butyltin dilaurate were heated in a water bath until the inner temperature of the flask became 70°C. Next, keeping the inner temperature of the flask at 70° C., while stirring the mixture, 161 g (1 mole) of 4-hydroxy-N-(2-hydroxyethyl)-N-methylbutyramide as the raw material of (b2) and (b3) 1326 g (1.5 mol) of polytetramethylene glycol (trade name: PTG850SN, manufactured by Hodogaya Chemical Industry Co., Ltd.) having a number average molecular weight of 877 (in terms of hydroxyl value) as a raw material was kept at 40° C. , using a dropping funnel with a side tube, it took 3 hours to drop at a constant rate. Fu...
Synthetic example 2
[0104] Synthesis of urethane acrylate mixture UA-2 (component (B))
[0105] In addition to using 80 g (0.5 mol) of 4-hydroxy-N-(2-hydroxyethyl)-N-methylbutyramide as the raw material of (b2), polystyrene with a number average molecular weight of 877 (in terms of hydroxyl value) was used as the raw material of (b3). Except 1768 g (2.0 mol) of tetramethylene glycols, it carried out similarly to the synthesis example 1, and obtained the urethane acrylate mixture UA-2.
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