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Fluorine-enhanced bioactive mineral powder and its preparation method and application

A bioactive mineral and mineral powder technology, applied in the field of oral medicine, can solve the problems of high equipment requirements, high production cost, and large loss of volatile phosphorus pentoxide, etc., and achieve the effect of shortening the hydration time and expressing the activity quickly

Active Publication Date: 2020-01-07
北京刷新活力健康科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, the melting temperature in the preparation process is high, resulting in a large loss of volatile phosphorus pentoxide. At the same time, the requirements for equipment are high, the production cost is high, and safety problems are prone to occur in the production process.

Method used

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  • Fluorine-enhanced bioactive mineral powder and its preparation method and application
  • Fluorine-enhanced bioactive mineral powder and its preparation method and application
  • Fluorine-enhanced bioactive mineral powder and its preparation method and application

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Example 1 A fluorine-enhanced bioactive mineral powder material and its preparation method

[0037] 1. The composition of the mineral powder material is:

[0038] Element mass percentage SiO 2

40％ CaO 25％ Na 2 o

23％ P 2 o 5

7％ F 5％

[0039] 2. Calculation of raw materials: Weigh various raw materials according to the following proportions:

[0040] Element mass percentage SiO 2

30％ CaCO 3

25％ Na 2 CO 3

30％ P 2 o 5

7％ sodium monofluorophosphate 8％

[0041] 3. Preparation method: Fully mix the above materials with mixing equipment. After mixing, put it into the crucible equipment. During the heating process of the crucible equipment, keep it at 650°C for 30 minutes, keep it at 700°C for 30 minutes, and finally keep it at 1050°C for 2 hours. After fully homogenizing, the mineral melt is put into pure water, rapidly quenched and cooled, and dried a...

Embodiment 2

[0043] Example 2 A fluorine-enhanced bioactive mineral powder material and its preparation method

[0044] The difference between this embodiment and embodiment 1 is: increase the consumption of sodium monofluorophosphate in the raw material to be 15%, reduce SiO in the raw material 2 The dosage is 23%.

[0045] After preparing according to the method described in Example 1, the composition of the obtained mineral powder material is:

[0046] Element mass percentage SiO 2

Embodiment 3

[0047] Example 3 A fluorine-enhanced bioactive mineral powder material and its preparation method

[0048] The difference between this embodiment and embodiment 1 is: increase the amount of sodium monofluorophosphate in the raw material to 10%, reduce the amount of CaCO in the raw material 3 The dosage is 20%.

[0049] After preparing according to the method described in Example 1, the composition of the obtained mineral powder material is:

[0050] Element mass percentage SiO 2

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Abstract

The invention relates to the field of dental medical treatment and in particular discloses fluorine-strengthened bioactivity mineral powder and a preparation method and an application thereof. The component system of constitution of the mineral powder is as follows: SiO-CaO-Na2O-P2O5-F. The powder comprises the following components in percentages by weight: 40-55% of SiO2, 15-30% of CaO, 15-30% of Na2O, 2-12% of P2O5 and 0.01-6% of F. According to the invention, by taking sodium monofluorophosphate as an importing components of fluorine element and controlling the mass ratio of sodium monofluorophosphate and phosphorus pentoxide added at 0.8-1.2, in a processing course, the loss of a volatile matter phosphorus pentoxide can be effectively reduced at a melting temperature of a material, so that calcium, phosphorus and fluorine in the material better meets a pre-designed proportion. By means of a shock chilling function of water, the amorphous state with more intermediate states is more easily formed, so that more crystal hydroxyapatite is formed during a reaction with water and is of higher activity. In the reaction process of the mineral powder and water, a phosphate component is further generated, thereby forming a better environment for generation of hydroxyapatite.

Description

technical field [0001] The invention relates to the field of oral medicine, in particular to a fluorine-enhanced bioactive mineral powder dental treatment. Background technique [0002] Dentin hypersensitivity (DH) is a common and frequently-occurring disease in the oral cavity. According to hydrodynamics, reducing the diameter of dentinal tubules and closing the openings of dentinal tubules to reduce and avoid fluid flow in dentin is the fundamental way to treat dentin sensitivity. The current treatment concept of anti-dentin hypersensitivity is gradually changing to early diagnosis and minimally invasive treatment, and the mineralization restoration treatment of dentinal tubules is well in line with this development trend. In long-term practice, it has been proved that apatite bioactive material and fluoride, as a traditional remineralization anti-caries substance, can also play a good role in sealing and repairing the defect of dentinal tubules. The repair process of de...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C12/00C03C6/06
CPCC03C1/00C03C12/00
Inventor 常丽李次会温承宇
Owner 北京刷新活力健康科技有限公司
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