A kind of preparation method of composite magnesium oxide powder for dental alginate impression material
A technology of magnesium oxide powder and dental alginate, applied in the direction of dental impression materials, magnesium oxide, dental preparations, etc., can solve the problem that the activity of a single magnesium oxide product is not well controlled and the performance indicators of magnesium oxide powder The requirements are not uniform, and it is difficult to accurately control the solidification time of the final impression material, so as to achieve the effect of accurate target solidification time, easy demolding, and complete impression
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Embodiment 1
[0032] A preparation method of composite magnesium oxide powder for dental alginate impression material, comprising the following steps:
[0033] (1) choose magnesium hydroxide powder raw material, wherein Mg(OH) 2 The content is 97.3%, CaO is 1.3%, SO 4 2- 0.3%, Cl - 0.10%, 9ppm for heavy metals, 2ppm for As, 0.08% for acid insolubles, 31.5% for loss on ignition, 1.8μm for laser particle size D50, and 96 for whiteness.
[0034] (2) Add the magnesium hydroxide powder raw material into the rotary kiln calciner, control the temperature range from the front part to the rear part in the rotary kiln to be 600°C to 625°C, and control the residence time of the material in the calciner to 1.4h . The magnesia powder after calcining was passed through a vibrating sieve to obtain a magnesia powder product A with 325 meshes passing through. The range of citric acid value for chemical detection of magnesium oxide A's reactivity is 145s, and the bulk density is 0.31g / cm 3 , The whiten...
Embodiment 2
[0041] A preparation method of composite magnesium oxide powder for dental alginate impression material, specifically comprising the following steps:
[0042] (1) choose magnesium hydroxide powder raw material, wherein Mg(OH) 2 98.0%, CaO 1.0%, SO 4 2- 0.42%, Cl - 0.11%, 8ppm for heavy metals, 3ppm for As, 0.09% for acid insolubles, 32% for loss on ignition, 1.6μm for laser particle size D50, and 97 for whiteness.
[0043] (2) Add the magnesium hydroxide powder raw material into the rotary kiln calciner, control the temperature range from the front part to the rear part in the rotary kiln to be 700°C to 740°C, and control the residence time of the material in the calciner to 1.2h . The magnesia powder after calcining was passed through a vibrating sieve to obtain a magnesia powder product A with 325 meshes passing through. The range of citric acid value for chemical detection of magnesium oxide A reactivity is 175s, and the bulk density is 0.34g / cm 3 , The whiteness of ...
Embodiment 3
[0050] A preparation method of composite magnesium oxide powder for dental alginate impression material, comprising the following steps:
[0051] (1) choose magnesium hydroxide powder raw material, wherein Mg(OH) 2 99.0%, CaO 0.5%, SO 4 2- 0.32%, Cl - 0.10%, 6ppm for heavy metals, 2ppm for As, 0.08% for acid insolubles, 31.5% for loss on ignition, 1.8μm for laser particle size D50, and 97 for whiteness.
[0052] (2) Add the magnesium hydroxide powder raw material into the rotary kiln calciner, control the temperature range from the front part to the rear part in the rotary kiln to be 520°C to 550°C, and control the residence time of the material in the calciner to 1.5h . The magnesia powder after calcining was passed through a vibrating sieve to obtain a magnesia powder product A with 325 meshes passing through. The range of citric acid value for chemical detection of magnesium oxide A reactivity is 125s, and the bulk density is 0.30g / cm 3 , The whiteness of glycosides ...
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