Ternary weeding composition containing C5H12NO4P

A herbicidal composition, refined glufosinate-ammonium technology, applied in the direction of herbicides and algicides, biocides, animal repellents, etc., can solve the loss, low effective utilization rate, grass weeds, broad-leaved weeds Grass and sedge weed susceptibility issues such as reduced

Inactive Publication Date: 2017-12-08
山东中新科农生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, chemical control is the leading measure for the control of weeds in farmland. The herbicides used to control grass weeds, broad-leaved weeds and sedge weeds are single-agent clopyralid, clopyralid and amilopyral Mainly, long-term single use can easily lead to decreased sensitivity of grass weeds, broad-leaved weeds and sedge weeds, resulting in resistance problems
[0006] In addition, pesticides, like chemical fertilizers, have a low effective utilization rate in the process of application, and a large amount of loss is one of the main reasons for the above-mentioned environmental hazards

Method used

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  • Ternary weeding composition containing C5H12NO4P
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  • Ternary weeding composition containing C5H12NO4P

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preparation example Construction

[0039] The preparation method of described modified chitosan comprises the following steps:

[0040] (1) Add N,N-dimethylformamide to the reactor, lower the temperature to 0-5°C, slowly add chlorosulfonic acid, stir for 0.5h, and obtain the sulfonating reagent, the N,N-dimethylformamide The weight ratio of amide to the chlorosulfonic acid is 1:3;

[0041] (2) Add chitosan to the reactor, the mass fraction is 2% dichloroacetic acid-formamide mixed solvent, stir for 0.5h, heat up to 60°C, add the sulfonating reagent in step (1), keep warm for 3h, cool down To room temperature, add dehydrated ethanol, the mass fraction of the chitosan and the 2% dichloroacetic acid-formamide mixed solvent, the sulfonating reagent, the weight ratio of the dehydrated ethanol is 1:5:4.2 : 10; filtered, washed 3 times with absolute ethanol, and dried under reduced pressure at 50° C. for 16 hours to obtain sulfonated chitosan;

[0042] (3) Add 1,7-diazo-12-crown-4 (CAS No.: 294-92-8) and absolute et...

Embodiment 1

[0069] The ternary herbicidal composition containing refined glufosinate-ammonium includes an active component and an adjuvant component, the active component is composed of refined glufosinate-ammonium, clopyralid, and acifluorfen, and the refined glufosinate-ammonium The mass ratio of phosphine to the clopyralid, the acifluorfen, and the acifluorfen is 20:5:1;

[0070] The wettable powder of the ternary herbicidal composition containing essence glufosinate-ammonium, calculated by weight percentage, includes:

[0071]

[0072] Wherein, the wetting agent is sodium lauryl sulfate, the dispersant is lignosulfonate (the lignosulfonate is calcium lignosulfonate), and the disintegrating agent is ammonium sulfate, The thickener is white carbon black, and the filler is modified chitosan; the modified chitosan is sulfonated chitosan grafted with azacrown ether and polyacrylamide;

[0073] The wettable powder preparation method of the ternary herbicidal composition containing essen...

Embodiment 2

[0083] The ternary herbicidal composition containing refined glufosinate-ammonium includes an active component and an adjuvant component, the active component is composed of refined glufosinate-ammonium, clopyralid, and acifluorfen, and the refined glufosinate-ammonium The mass ratio of phosphine to the clopyralid, the acifluorfen, and the acifluorfen is 20:5:1;

[0084] The wettable powder of the ternary herbicidal composition containing essence glufosinate-ammonium, calculated by weight percentage, includes:

[0085]

[0086]

[0087] Wherein, the wetting agent is sodium lauryl sulfate, the dispersant is lignosulfonate (the lignosulfonate is calcium lignosulfonate), and the disintegrating agent is ammonium sulfate, The thickener is white carbon black, and the filler is modified chitosan; the modified chitosan is sulfonated chitosan grafted with azacrown ether and polyacrylamide.

[0088] The preparation method of the wettable powder of the ternary herbicidal compositi...

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Abstract

The invention provides ternary weeding composition containing C5H12NO4P. The ternary weeding composition containing C5H12NO4P comprises an active component and an auxiliary component, wherein the active component is prepared from C5H12NO4P, clopyralid and fluoroglycofen-ethyl in the mass ratio being (10-30): (1-10):1.

Description

technical field [0001] The invention belongs to the application field of agricultural chemicals, in particular, the invention relates to a ternary herbicidal composition containing refined glufosinate-ammonium. Background technique [0002] The chemical formula of glufosinate ammonium is C 5 h 12 NO 4 P, the formula weight is 181.27, the chemical name is 4-[hydroxyl (methyl)phosphono]-L-homoalanine, it is L-type glufosinate-ammonium, it is easily soluble in water, not easily soluble in organic solvents, and is suitable for light Stable, melting point 214-216 ℃, is a highly efficient, low toxicity, non-selective contact type phosphoric acid herbicide. The refined glufosinate-ammonium is an L-type glufosinate-ammonium, and its herbicidal activity is twice that of the racemic DL-type glufosinate-ammonium mixture. Glufosinate-ammonium inhibits glutamine synthetase, leading to nitrogen metabolism disorder in plants, accumulated ammonia poisoning, and then chloroplast synthesi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N57/20A01N43/40A01N37/48A01P13/00
CPCA01N37/48A01N43/40A01N57/20
Inventor 王世辉李路路
Owner 山东中新科农生物科技有限公司
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