Composition for fingerprint imaging and its application
A composition and fingerprint technology, applied in the fields of application, medical science, diagnosis, etc., can solve the problem of inapplicable objects of similar colors, and achieve the effect of excellent fingerprint imaging effect, good adhesion and wide applicability.
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Embodiment 1
[0090] Example 1. Preparation and Fingerprint Imaging of Silica-Tetraphenylethylene (TPE) Composition
[0091] 600 mesh silicon dioxide (SiO 2 ) powder and TPE were dissolved in dichloromethane (DCM) according to different weight ratios (respectively 20:1, 30:1, 40:1 and 50:1), treated under 40kHz, 185W ultrasound for 10 minutes, and then used Rotary evaporator was dried at 30-40°C to obtain silica-tetraphenylethylene (SiO 2 - TPE) powder, the particle size of the powder is 300-400 mesh.
[0092] Then SiO 2 - TPE powder is brushed from one direction to the other to show the standard fingerprint on the glass slide (the term "standard fingerprint" is a conventional technical term in the field of fingerprint imaging, which refers to the fingerprint whose mastoid line meets the following nine detailed features: starting point, end point, divergence, combination, small ditch, small bridge, small eye, small stick, small point). Under the daylight and 365nm band hand-held UV lamp...
Embodiment 2
[0093] Example 2. SiO 2 -TPE, SiO 2 -TPE-4OMe, SiO 2 -TPE-OBu, SiO 2 - Preparation of TPA-TPE and its comparison with commercially available blue fluorescent powder
[0094] All SiO 2 -AIE powder is prepared in the same manner as in Example 1, wherein silicon dioxide (SiO 2 ) The particle size of the powder is 300-400 mesh, SiO 2 The weight ratio to TPE, TPE-4OMe, and TPE-OBu is 30:1, and the particle size of the prepared powder is 300-400 mesh.
[0095] According to the method of embodiment 1 SiO 2 -TPE, SiO 2 -TPE-OBu and SiO 2 -TPE-4OMe applied over standard fingerprints on glass slides. Imaging results such as figure 2 shown. As can be seen from the bright field images, SiO 2 - Adhesion of TPE-4OMe is better than that of SiO 2 - TPE is better, and the fluorescence imaging effect is better than SiO 2 -TPE is better. The bright field imaging effect of TPE-OBu is also relatively good, and the fluorescence imaging effect is very clear. This demonstrates that a...
Embodiment 3
[0097] Example 3. Preparation and comparative experiments of Mag, Mag-TPE, Mag-TPA-TPE, Mag-Silo-OMe, Mag-DPA-IQ, Mag-DPI-B, Mag-TPA-TPP, Mag-TFE
[0098] Mag-TPE, Mag-TPA-TPE, Mag-Silo-OMe, Mag-DPA-IQ were prepared by mixing different types of AIE molecules with magnetic powder (Mag) (purchased from Beijing Finger Technology Co., Ltd., D008) , Mag-DPI-B, Mag-TPA-TPP and Mag-TFE powders, the preparation method is carried out as described in Example 1, wherein the weight ratio of magnetic powder to the above-mentioned AIE molecules is 100:1, and the particle size of the obtained powder is 300- 400 mesh. Silo-OMe is a highly fluorescent green AIE molecule with short aliphatic chains, DPA-IQ is an orange-red AIE molecule with positive charges, and DPI-B, TPA-TPP, and TFE are AIE molecules with different core structures.
[0099] Apply Mag, Mag-TPE, Mag-TPA-TPE, Mag-Silo-OMe, Mag-DPA-IQ, Mag-DPI-B, Mag-TPA-TPP and Mag-TFE to the glass guest according to the method of Example 1 o...
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