A method for preparing an all-hydrogel stretchable supercapacitor and the capacitor
A technology for supercapacitors and hydrogels, applied in hybrid capacitor electrodes, hybrid capacitor electrolytes, hybrid/electric double layer capacitor manufacturing, etc., can solve the problem that the substrate does not make any contribution to the electrochemical energy storage of supercapacitors, electrode materials and elastic substrates Stretchability does not match, active materials cannot be distributed ideally and continuously, etc., to achieve good charge-discharge cycle stability, excellent electrochemical properties, and good stretchability
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[0037] figure 1 It is a schematic diagram of the design principle of preparing an all-hydrogel stretchable supercapacitor constructed according to the present invention, and the stretchable supercapacitor is assembled entirely from hydrogel materials. Such as figure 1 As shown in , the preparation process mainly includes the following process steps:
[0038] S1 First, the dilution of carbon nanotubes (CNTs)
[0039] Weigh the CNT water-based slurry, add deionized water, stir first, and then sonicate.
[0040] In this step, the commercially available CNT water-based slurry with a mass fraction of 5% can be added to deionized water, stirred first, and then ultrasonicated. Specifically, the stirring time is preferably set at 6h-10h, and the stirring speed is preferably set at 200-500r / min until the mixed solution is stirred into a uniform ink-like solution; then it is ultrasonically 60min-120min, more preferably 90min , to obtain a dilute solution of the CNT water-based dispe...
Embodiment 1
[0055] Weigh acrylamide, dissolve acrylamide in the diluted aqueous dispersion of CNT with a mass fraction of 2%, stir evenly, then weigh sodium alginate, slowly add it to the mixture, and stir at room temperature for 8 hours until it forms Uniform CNT / AM / SA mixed solution, the mass fraction of acrylamide in the uniform CNT / AM / SA mixed solution is 17%, the mass fraction of sodium alginate is 2%; The AM / SA mixture was mixed with PEDOT / PSS (model PH1000), stirred at room temperature for 2 h, and then 0.01% of the cross-linking agent N,N-methylenebisacrylamide was added sequentially, and the mass fraction of 0.09% The catalyst tetramethylethylenediamine and the initiator ammonium persulfate with a mass fraction of 0.1% are mixed evenly, and the mixed solution is quickly transferred to a clean petri dish, and left to stand for 6 hours until the polymerization reaction is complete; The petri dish was sealed and then placed in a drying oven at 80°C for 12 hours to complete the polym...
Embodiment 2
[0059] Weigh acrylamide, dissolve the acrylamide in the diluted aqueous dispersion of CNT with a mass fraction of 2%, stir evenly, then weigh sodium alginate, slowly add it to the mixture, and stir at room temperature for 8 hours until Form a uniform CNT / AM / SA mixed solution, the mass fraction of acrylamide in the uniform CNT / AM / SA mixed solution is 16%, the mass fraction of sodium alginate is 3%; / AM / SA mixture mixed with PEDOT / PSS (model PH1000), stirred at room temperature for 3 hours, and then sequentially added 0.02% of cross-linking agent N,N-methylenebisacrylamide with a mass fraction of 0.1% The catalyst tetramethylethylenediamine and the initiator ammonium persulfate with a mass fraction of 0.1% are mixed evenly, and the mixed solution is quickly transferred to a clean petri dish, and left to stand for 6 hours until the polymerization reaction is complete; The complete petri dish is sealed and then placed in a drying oven at 70°C for 12 hours to complete the polymeriz...
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