Low-temperature sintered microwave dielectric ceramic material and preparation method thereof
A technology of microwave dielectric ceramics and low-temperature sintering, applied in the field of functional ceramics, can solve the problems of large dielectric loss and small Qf value, and achieve the effect of no pollution in the process, simple process and broad application prospects
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Embodiment 1-8
[0035] Using chemical raw material Bi with a purity greater than 99.9% 2 o 3 、WO 3 , TeO 2 Preparation of BiW 0.5 Te 3 o 12 Microwave dielectric ceramics, the specific implementation is as follows:
[0036] (1) will Bi 2 o 3 、WO 3 , TeO 2 Weigh the ingredients according to the molar ratio of 1:0.5:3, specifically weigh 3.9908 grams of Bi 2 o 3 , 1.9856 g WO 3 , 9.0236 g TeO 2 After mixing, the raw materials are added to the nylon tank, and ball milled for 4 to 6 hours. The specific ball milling time of Examples 1-8 is shown in Table 1; the ball milled raw materials are placed in an infrared drying oven to dry and sieve;
[0037] (2) Calcining the sieved raw materials at 400° C. for 3 hours;
[0038] (3) adding a mass percentage of 5% PVA aqueous solution to the calcined powder for granulation, sieving after drying, and pressing into a cylindrical shape of Φ12mm×6mm with a powder tablet press;
[0039] (4) sintering the cylinder of step (3) at 480-530° C., and ke...
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