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A kind of preparation method of perilla flavoring for tobacco and its application in cigarette

A perilla seed and spice technology, which is applied in the field of preparation of perilla spice for cigarettes, to achieve complete leaching, good application effect, and high solvent utilization rate

Active Publication Date: 2020-10-23
CHINA TOBACCO GUANGXI IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is no use of membrane separation technology to separate perilla extract to prepare tobacco spices

Method used

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  • A kind of preparation method of perilla flavoring for tobacco and its application in cigarette
  • A kind of preparation method of perilla flavoring for tobacco and its application in cigarette
  • A kind of preparation method of perilla flavoring for tobacco and its application in cigarette

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Take the dried perilla seed medicinal material, pulverize it into a coarse powder, and pass it through a 10-mesh stainless steel screen; accurately weigh the perilla seed powder, put it in a percolation drum, add 11 times the amount of 65% ethanol, soak it for 24 hours after wetting; Extract by percolation at a speed of 5mL / min until the percolation solution with a mass of 10 times the mass of the coarse powder of medicinal materials is obtained, then stop the extraction and filter the percolation solution for later use; take percolation hydraulic distillation until no ethanol flows out to obtain perilla seed extract.

[0030] Accurately weigh the perilla extract and place it in a quantitative glass container, add 50 times the amount of 20% ethanol to dissolve, and the dissolved solution is D1. After the dissolution is complete, use a 50nm ceramic microfiltration membrane to filter, and the cut-off section is D2; the permeate liquid of the microfiltration membrane is fil...

Embodiment 2

[0033] Take the dried perilla seed medicinal material, pulverize it into a coarse powder, and pass it through a 10-mesh stainless steel screen; accurately weigh the perilla seed powder, place it in a percolation drum, add 20 times the amount of 50% ethanol, soak it for 24 hours after wetting; Percolation extraction at a speed of 2mL / min, until the percolation liquid with a mass of 18 times the mass of the coarse powder of medicinal materials was obtained, the extraction was terminated, and the percolation liquid was filtered for later use; the percolation liquid was hydraulically distilled until no ethanol flowed out to obtain perilla seed extract.

[0034] Accurately weigh the perilla extract and place it in a quantitative glass container, add 50 times the amount of 20% ethanol to dissolve, and the dissolved solution is D1. After the dissolution is complete, use a 200nm ceramic microfiltration membrane to filter, and the cut-off section is D2; the permeate liquid of the microf...

Embodiment 3

[0037] Take the dried perilla seed medicinal material, pulverize it into a coarse powder, and pass it through a 10-mesh stainless steel screen; accurately weigh the perilla seed powder, place it in a percolation drum, add 5 times the amount of 95% ethanol, soak it for 24 hours after wetting; Extract by percolation at a speed of 10mL / min, until the percolation solution with a mass four times the mass of the coarse powder of medicinal materials is obtained, the extraction is terminated, and the percolation solution is filtered for later use; the percolation fluid is hydraulically distilled until no ethanol flows out to obtain perilla seed extract.

[0038] Accurately weigh the perilla extract and place it in a quantitative glass container, add 50 times the amount of 20% ethanol to dissolve, and the dissolved solution is D1. After the dissolution is complete, use a 100nm ceramic microfiltration membrane to filter, and the cut-off section is D2; the permeate liquid of the microfilt...

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PUM

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Abstract

The invention provides a preparation method of fructus perillae spice used for a cigarette. A dry fructus perillae medicinal material is subjected to smashing, screening, ethyl alcohol is steeped for24 h and subjected to percolation extraction at a certain flow rate to obtain a certain amount of percolation extraction liquid, and filtering and concentration are conducted to obtain a fructus perillae extract; the fructus perillae extract is dissolved in ethyl alcohol, and ceramic microfiltration membrane is used for filtering out macromolecular substances; microfiltration membrane permeate isfiltered by an organic ultrafiltration membrane to filter out part of micromolecule substances which affect the aroma and the taste, and the part intercepted by the organic ultrafiltration membrane issubjected to reduced pressure distillation and concentration to obtain the fructus perillae spice used for the cigarette. The invention further provides application of the spice in the cigarette; thefructus perillae spice used for the cigarette is diluted and sprayed onto cut tobacco according to a certain ratio, and through rolling, the cigarette is prepared. After the spice is added, the richness and the thick texture of the cigarette aroma can be obviously improved, the air feeling and the smooth feeling of smoke are improved, the moistening feeling is improved, and irritation and offensive odor can be reduced, so that the smoke is soft, and the remaining taste is comfortable.

Description

Technical field: [0001] The invention belongs to the technical field of preparation of tobacco additives, and in particular relates to a preparation method of tobacco perilla spice and its application in cigarettes. [0002] technical background: [0003] Zisuzi is the dry and ripe fruit of perilla, a plant of the Labiatae family. Multi-line cultivation. Mainly produced in Gansu, Hubei, Jiangsu, Hunan, Zhejiang, Anhui, Henan and other places. Perilla seed is one of the commonly used traditional Chinese medicines, with pungent taste and warm nature. Return lung meridian. Efficacy Lowering qi and reducing phlegm, relieving cough and asthma, moistening intestines. The clinical names are perilla seeds, fried perilla seeds, honey roasted perilla seeds, and perilla seeds cream. The application of perilla seed in tobacco flavoring has not been reported. Our laboratory is engaged in the research and development of perilla flavoring for tobacco, but although the conventionally p...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00A24B15/30
CPCA24B15/302C11B9/00
Inventor 吴彦黄东业胡志忠宋凌勇陈义昌刘鸿李志华农李政宁振兴徐石磊杨龙彦廖超执黄江锋黄善松胡超班强务文涛
Owner CHINA TOBACCO GUANGXI IND
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