Borate type automobile brake fluid

A technology of automobile brakes and borates, which is applied in the petroleum industry, additives, lubricating compositions, etc., can solve the problems of increasing the steric hindrance of borates, reducing the temperature rise of brake fluid, and volatile moisture, etc., and achieves good Effect of Low Temperature Kinematic Viscosity

Inactive Publication Date: 2018-12-21
张家港迪克汽车化学品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Chinese patent CN 03111223.4 relates to a motor vehicle brake fluid and its production method, and discloses a method of producing brake fluid from a polymer mixture produced by diethylene glycol and 1,1-dichloroethane under the action of a catalyst. method, but the DOT4 brake fluid technical indicators described in the patent can only meet the general standard requirements, and there is still a big gap from the technical indicators of the super DOT4 brake fluid and DOT5.1 brake fluid required by some automobile manufacturers. Its low-temperature kinematic viscosity at -40°C reaches 1217mm 2 /s, it cannot meet the requirement of DOT5.1 brake fluid ≤900mm 2 /s technical requirements, let alone meet the requirements of DOT6 ≤750mm 2 The specification of /s requires a
[0006] Chinese patent CN201611072418.9 relates to a brake fluid, which includes the following raw materials in mass percentage: 40% to 50% of deionized water, 38% to 55% of antifreeze, 0.5% to 1.5% of stabilizer, and 1.5% of antioxidant % to 3%, preservative 1% to 4%, passivator 2% to 3.5%, the brake fluid of the present invention effectively reduces the temperature rise of the brake fluid, and weakens electrochemical corrosion, effectively meeting the requirements of large Energy-level brakes have strict requirements on the performance of brake fluid, but the brake fluid described in the brake fluid technology of this invention is

Method used

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  • Borate type automobile brake fluid

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Experimental program
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Effect test

Embodiment 1

[0022] Into a 1.5T reactor, add polyethylene glycol butyl ether composition: 80kg; polyethylene glycol methyl ether composition: 78kg; triethylene glycol methyl ether borate: 834kg; start adding additives after stirring for 5 minutes, Each additive is added at an interval of 5 minutes and then the next adjuvant is added in order, 6-methyl-2-mercaptobenzothiazole: 0.3kg; methylbenzotriazole: 0.35kg; antioxidant BHT: 0.6kg ; 2-ethylhexyl acrylate: 0.15kg; 4,4′-butylene bis(6-tert-butyl m-cresol): 0.12kg; 2,2-【【(methyl-1H-benzotri Azol-1-yl)methyl]imino]Diethanol: 1.1kg; methylparaben: 0.02kg; dodecahydrodiphenylamine: the rest; each material is added at an interval of 5min, and after stirring for 6h, it can pass 0.1 The um filter is filtered and sub-packed to obtain borate type automobile brake fluid.

Embodiment 2

[0024] In a 1.5T reactor, add polyethylene glycol butyl ether composition: 54kg; polyethylene glycol methyl ether composition: 54kg; triethylene glycol methyl ether borate: 884kg; start adding additives after stirring for 5 minutes, Each additive is added at an interval of 5 minutes and then the next adjuvant is added in order, 6-methyl-2-mercaptobenzothiazole: 0.4kg; methylbenzotriazole: 0.45kg; antioxidant BHT: 0.7kg ; 2-ethylhexyl acrylate: 0.16kg; 4,4'-butylene bis(6-tert-butyl m-cresol): 0.15kg; 2,2-【【(methyl-1H-benzotri Azol-1-yl)methyl]imino]Diethanol: 1.0kg; ethyl paraben: 0.01kg; dodecahydrodiphenylamine: the rest; each material is added at an interval of 5min, and after stirring for 6h, it can pass 0.1 The um filter is filtered and sub-packed to obtain borate type automobile brake fluid.

Embodiment 3

[0026] Add polyethylene glycol butyl ether composition: 62kg; triethylene glycol methyl ether borate: 930kg into a 1.5T reaction kettle; start adding additives after stirring for 5 minutes, and add each additive in sequence after 5 minutes. The next adjuvant, 6-methyl-2-mercaptobenzothiazole: 0.25kg; methyl benzotriazole: 0.25kg; antioxidant BHT: 0.7kg; 2-ethylhexyl acrylate: 0.3 kg; 4,4'-butylene bis(6-tert-butyl m-cresol): 0.2kg; 2,2-[[(methyl-1H-benzotriazol-1-yl)methyl] imino 】Diethanol: 1.5kg; methyl paraben: 0.015kg; tri-n-butylamine: the rest; each material is added at an interval of 5 minutes, and after stirring for 6 hours, it can be filtered and packed through a 0.1um filter to obtain borate Type car brake fluid.

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Abstract

The invention discloses a borate type automobile brake fluid. The borate type automobile brake fluid is prepared from the following components in percentage by mass: 0 to 15 percent of polyethylene glycol ether composition, 80 to 97 percent of triethylene glycol methyl ether borate, 0.02 to 0.15 percent of 6-methyl-2-mercaptobenzothiazole, 0.02 to 0.15 percent of methyl benzotriazole, 0.05 to 0.20percent of antioxidant BHT, 0.01 to 0.20 percent of acrylic acid-2-ethylhexyl ester, 0.01 to 0.05 percent of 4,4'-butylenebis(6-tert-butylm-cresol). 0.05 to 0.5 percent of 2,2-[methyl-1H-benzotriazole-1-yl]methyl]imino]diethanol, 0.001 to 0.05 percent of nipagin ester and 0.3 to 1.0 percent of alkalinity regulator, wherein the polyethylene glycol ether composition is one or a combination of polyethylene glycol monomethyl ether and polyethylene glycol monobutyl ether. The brake fluid disclosed by the invention meets the requirement of higher dry-wet boiling point, and has excellent low-temperature driving performance, thereby making braking more sensitive and driving safe.

Description

Technical field [0001] The invention relates to the technical field of brake fluids for automobile brake systems, in particular to a borate type automobile brake fluid. Background technique [0002] Since the 1970s, a new generation of synthetic brake fluids with higher dry and wet boiling points, lower low-temperature kinematic viscosity and low water sensitivity have become a research focus in various countries. Subsequently, automobile brake fluids have been extensively developed. At present, the mainstream products in the world are DOT4 and DOT5.1 brake fluids with alcohol ether borate as the main raw material, and the newly launched DOT6 brake fluid. DOT4 borate type synthetic brake fluids are already in the world It has been widely used. The use of DOT5.1 type brake fluid is less, the main reason is its higher price. For DOT6 brake fluid, its cost is controllable, and its low temperature performance is more excellent, which can be widely used. To meet the needs of ABS brak...

Claims

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Application Information

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IPC IPC(8): C10M163/00C10N30/02C10N30/12
CPCC10M163/00C10M2207/026C10M2207/144C10M2207/281C10M2209/104C10M2209/108C10M2215/04C10M2215/044C10M2215/064C10M2215/223C10M2219/104C10M2227/061C10N2030/02C10N2030/12
Inventor 陶佃彬邹密单猛杨飞
Owner 张家港迪克汽车化学品有限公司
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