Portable AHL molecular imprinting silk-screen printing electrochemical detector
A technology of screen printing electrodes and molecular imprinting, applied in the direction of material electrochemical variables, etc., can solve the problems of large number of molecularly imprinted membranes and waste of resources, and achieve the effects of high specificity, increased sensitivity, and increased electron transfer rate.
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Embodiment 1
[0047] Example 1 Preparation of AHL Molecularly Imprinted Screen Printing Electrode
[0048] The schematic diagram of the preparation of AHL molecularly imprinted screen-printed electrode sheet is as follows figure 1 shown. The specific preparation method is as follows:
[0049] (1) Drop gold nano-crosses on the surface of the working screen printing electrode, drip coating method: drip-coat the configured gold nano-crosses solution on the surface of the working electrode, and dry it under an infrared lamp to complete the dripping of the gold nano-crosses add. The peak current value of the electrode on the CV diagram can be increased by dripping the gold nano cross, that is, the sensitivity of the electrode can be increased, such as image 3 shown.
[0050] (2) Modification of p-mercaptoaniline through gold sulfhydryl bonds, modification method: dip the screen-printed electrode coated with gold nanoparticles in a 50 mmol L-1 ethanol solution of p-mercaptoaniline, soak at r...
Embodiment 2
[0053] Example 2 Portable AHL Molecularly Imprinted Screen Printing Electrochemical Detector
[0054] The structure diagram of the portable AHL molecular imprinting electrochemical detector is as follows figure 2 As shown, the structure is as follows:
[0055] The molecularly imprinted screen-printed electrode obtained in Example 1 includes an electrode substrate, a terminal, an electrode connection, a working electrode, a counter electrode, and an insulating layer; the surface of the working electrode is electroplated with a molecularly imprinted polymer film; the electrode substrate is a primary The consumer substrate, working electrode, counter electrode and reference electrode are derived from the electrode connection to form a convex three-wire socket, which can be inserted into a portable electrochemical detector for detection and reading. The electrode substrate is printed with an electrode base body in which connecting terminals, electrode connecting wires and workin...
Embodiment 3
[0059] Example 3 standard curve
[0060] In a portable detector of the present invention, which is a dedicated portable detector for AHL, the standard curve between AHL concentration and peak current difference has been built into the detector program.
[0061] The drawing method of this standard curve: prepare different known concentrations (concentration range: 1 * 10 -13 ~1×10 -9 mol L -1 )’s AHL molecularly imprinted screen-printed electrode is inserted into the detector to detect the current peak value formed when electrons flow from the counter electrode, through the conductive liquid, and then flow back to the workstation from the working electrode. Take the AHL concentration as the abscissa, and the peak current value as the ordinate Coordinates, the standard curve is obtained, such as image 3 shown. The standard curve equation that obtains is: y=0.56439lgx+8.57752 (R 2 =0.94799), the detection limit was 10 -11 mol L -1 .
[0062] The obtained standard curve i...
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