Hindered phenol antioxidant and synthesis method thereof
A technology for antioxidants and hindered phenols, which is applied in the field of hindered phenolic antioxidants and their synthesis, can solve the problems of single antioxidant properties and poor use effect, and can shorten the synthesis time, improve the use effect, and strengthen the tensile property. and the effect of bending resistance
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Embodiment 1
[0025] An embodiment of the present invention provides a hindered phenolic antioxidant, which consists of the following parts by weight: 10 parts of 2,6-di-tert-butyl-p-nitrophenol, 0.3 parts of potassium hydroxide, 0.1 parts of ferric chloride 50 parts of absolute ethanol, 3 parts of organic zinc, 1 part of phosphite compound, 4 parts of light stabilizer.
[0026] Wherein organic zinc is selected from zinc gluconate or zinc methionine; Phosphite compounds are pentaerythritol distearyl diphosphite, two (2,4-di-tert-butylphenyl) pentaerythritol phosphite, three-(2 , one or more of 4-di-tert-butylphenol) phosphite; light stabilizers are triazines, substituted acrylonitriles, oxalamides, salicylates, benzophenones, benzene One or more of triazoles.
[0027] A kind of synthetic method of hindered phenolic antioxidant, comprises the following steps:
[0028] S1. Prepare 2,6-di-tert-butyl-p-nitrophenol, potassium hydroxide, ferric chloride, absolute ethanol, organic zinc, phosphit...
Embodiment 2
[0033] An embodiment of the present invention provides a hindered phenolic antioxidant, which consists of the following parts by weight: 20 parts of 2,6-di-tert-butyl-p-nitrophenol, 0.6 parts of potassium hydroxide, 0.2 parts of ferric chloride 75 parts of absolute ethanol, 3.5 parts of organic zinc, 1.5 parts of phosphite compounds, and 5 parts of light stabilizer.
[0034] Wherein organic zinc is selected from zinc gluconate or zinc methionine; Phosphite compounds are pentaerythritol distearyl diphosphite, two (2,4-di-tert-butylphenyl) pentaerythritol phosphite, three-(2 , one or more of 4-di-tert-butylphenol) phosphite; light stabilizers are triazines, substituted acrylonitriles, oxalamides, salicylates, benzophenones, benzene One or more of triazoles.
[0035] A kind of synthetic method of hindered phenolic antioxidant, comprises the following steps:
[0036] S1. Prepare 2,6-di-tert-butyl-p-nitrophenol, potassium hydroxide, ferric chloride, absolute ethanol, organic zinc...
Embodiment 3
[0041] An embodiment of the present invention provides a hindered phenolic antioxidant, which consists of the following parts by weight: 30 parts of 2,6-di-tert-butyl-p-nitrophenol, 0.9 parts of potassium hydroxide, 0.3 parts of ferric chloride 100 parts of absolute ethanol, 4 parts of organic zinc, 2 parts of phosphite compounds, and 6 parts of light stabilizer.
[0042] Wherein organic zinc is selected from zinc gluconate or zinc methionine; Phosphite compounds are pentaerythritol distearyl diphosphite, two (2,4-di-tert-butylphenyl) pentaerythritol phosphite, three-(2 , one or more of 4-di-tert-butylphenol) phosphite; light stabilizers are triazines, substituted acrylonitriles, oxamides, salicylates, benzophenones, benzene One or more of triazoles.
[0043] A kind of synthetic method of hindered phenolic antioxidant, comprises the following steps:
[0044] S1. Prepare 2,6-di-tert-butyl-p-nitrophenol, potassium hydroxide, ferric chloride, absolute ethanol, organic zinc, pho...
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