Organic-inorganic compound for long-acting microorganism protection and preparation method thereof
An inorganic compound and microbial technology, applied in botany equipment and methods, chemicals for biological control, biocides, etc., can solve problems such as damage to sprayed objects, improper dilution concentration, fire, etc., to achieve Prolong the action time, avoid waste, and avoid the effect of migration
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[0034] In some preferred embodiments, the preparation method of acid-modified bentonite refers to the following steps:
[0035] 1) Add bentonite to the flask, then add sulfuric acid aqueous solution, add a condensing device, control the reaction temperature to 70-90°C, and heat in a water bath for 5-10 hours to obtain a mixture;
[0036] 2) centrifuge the mixture after the reaction in step 1), pour out the supernatant, add water to the precipitate in the centrifuge tube and stir to continue centrifugation until there is no sulfate ion in the supernatant (check with a saturated barium chloride aqueous solution until there is no precipitate generate);
[0037] 3) The precipitate obtained in step 2) is taken out, dried, ground, and set aside.
[0038] In some preferred embodiments, the molar concentration of the sulfuric acid aqueous solution in step 1) is 2-6 mol / L.
[0039] In some preferred embodiments, the molar concentration of the sulfuric acid aqueous solution described ...
Embodiment 1
[0089] An organic-inorganic compound for long-term protection against microorganisms. The preparation raw materials are calculated in parts by weight, including: 50 parts of polymer materials, 0.5 parts of coupling agents, 0.1 parts of emulsifiers, 0.5 parts of chelating agents, 1 part of organic antibacterial agents, inorganic 10 parts of antibacterial agent, 150 parts of solvent.
[0090] The polymer material is polyethylene glycol modified cyclodextrin.
[0091] The preparation method of described polyethylene glycol modified cyclodextrin refers to the following steps:
[0092] Add 20g of cyclodextrin into water, control the temperature to 75°C, then add 50g of polyethylene glycol, mix and stir for 4 hours, cool down to 23°C, let stand, filter, and dry the obtained solid to obtain the product.
[0093] Polyethylene glycol, model cx190, was purchased from Shandong Chuxin Chemical Co., Ltd.; cyclodextrin was purchased from Shandong Fuhe Biotechnology Co., Ltd.
[0094] The ...
Embodiment 2
[0116] An organic-inorganic compound for long-term protection against microorganisms. The preparation raw materials are calculated in parts by weight, including: 100 parts of polymer materials, 5 parts of coupling agents, 1 part of emulsifiers, 3 parts of chelating agents, 10 parts of organic antibacterial agents, inorganic 1 part of antibacterial agent, 200 parts of solvent.
[0117] The polymer material is polyethylene glycol modified cyclodextrin.
[0118] The preparation method of described polyethylene glycol modified cyclodextrin refers to the following steps:
[0119] Add 20g of cyclodextrin into water, control the temperature at 75°C, then add 50g of polyethylene glycol, mix and stir for 4 hours, cool down to 23°C, let stand, filter, and dry the obtained solid to obtain the product.
[0120] Polyethylene glycol, model cx190, was purchased from Shandong Chuxin Chemical Co., Ltd.; cyclodextrin was purchased from Shandong Fuhe Biotechnology Co., Ltd.
[0121] The coupli...
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