Porous photocatalysis and production thereof
A photocatalyst and porosity technology, applied in the direction of catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc., can solve problems such as ignoring operability and economy, and difficult to control moisture content
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Embodiment 1
[0011] Embodiment 1 (preparation method of hydrogel)
[0012] Two solutions of 100 parts by weight of sulfuric acid (20% by weight) and 100 parts by weight of sodium silicate (24 degrees Baume) were mixed and reacted, and washed with water to obtain a hydrogel. Dry the hydrogel, adjust the water content, and classify. At this time, it is best to keep the water content of the hydrogel between 30% and 80%. Especially when it is about 60%, it is the most productive and economical.
Embodiment 2
[0013] Embodiment 2 (preparation method of photocatalyst sol)
[0014] Dilute 60 g of titanium tetraisopropoxide with 500 ml of absolute ethanol. While stirring, 20 grams of diethanolamine and 5 grams of water were added. Then add 5 grams of polyethylene glycol with a molecular weight of 1000 to prepare a transparent sol.
Embodiment 3
[0015] Embodiment 3 (preparation method 1 of porous photocatalyst)
[0016] Put the hydrogel synthesized in Example 1 into the photocatalyst sol prepared in Example 2 and soak for 5 minutes, take it out, fully remove the photocatalyst sol, and dry at 170°C. Then the temperature is raised to 500°C for sintering, so that the crystal form of titanium dioxide is converted from rutile to anatase, thereby obtaining a porous photocatalyst.
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