Purifying solid substance by zone heating and smelting and molecule spreading method, and its device
A technology of molecular diffusion and regional heating, which is applied in the field of arsenic removal from yellow phosphorus, can solve the problems of low recovery rate, no conventional solvent for yellow phosphorus, complicated operation, etc.
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[0125] The present invention will be described in the form of specific implementation below. However, the data of the examples should not be construed as any implicit or obvious limitation to the scope of the present invention.
[0126] The device of the embodiment
[0127] The device of the embodiment is in figure 1 show. Because phosphorus is flammable, all operations must be done underwater. The dimensions of the apparatus of the example are 60x42x30 (cm).
[0128] The heater is shown on image 3 . All components are in image 3 There are instructions. For a steady movement of the heater over the sample rod, eg a speed-controlled motor can be used.
[0129] The heater is the most important part. It is an electric heating wire wrapped around an aluminum tube. The aluminum tube wrapped with the heating wire is integrally embedded in the plastic block (as follows Figure 4shown). There is a thermocouple in the center of the heater to control the temperature of the...
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