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Transparent anadate glass with high gain coefficient and preparing method thereof

A vanadate, high-gain technology, applied in the field of transparent vanadate glass, can solve the problem of unsatisfactory gain coefficient and achieve the effect of high gain coefficient

Inactive Publication Date: 2005-02-23
FUDAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The inventor once proposed a transparent vanadate glass whose basic composition is V 2 o 5 -SiO 2 -MO--X 2 O, where MO is (CaO+BaO+SrO), X 2 O is (Na 2 O+K 2 O+Cs 2 O), this vanadate glass has good light transmission performance, but its gain coefficient is not ideal enough (seeing Chinese Patent Application No. 200410018232.9)

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] According to the following main substance anion mass percentage V 2 o 5 : 22%; SiO 2 : 28%; Na 2 O: 5%; K 2 O: 10%; Cs 2 O: 5%; CaO: 12%, BaO: 18%, Nd 2 o 3 It is 0.8% of the total amount of the former. Weigh the vanadate glass raw material, mix it evenly, add it into a platinum crucible, melt it at 1400°C for 2 hours in dry oxygen with a concentration of more than 99%, and cast it into a mold. Cool in the annealing box from (Tg+10)°C to (Tg-100)°C at a rate of 1°C per hour, then take it out and cool it naturally. After cutting and polishing, the desired transparent vanadate glass can be obtained. After measurement, its stimulated emission cross section is 4.2pm 2 .

Embodiment 2

[0015] According to the following main substance anion mass percentage V 2 o 5 : 31%; SiO 2 : 19%; Na 2 O: 5%; K 2 O: 16%; CaO: 7%, BaO: 11%: SrO: 11%, Nd 2 o 3 It is 5% of the total amount of the former. Weigh the vanadate glass raw material, mix it evenly, add it into a platinum crucible, melt it at 1350°C for 2.5 hours in dry oxygen with a concentration of more than 99%, and cast it into a mold. Cool in the annealing box from (Tg+10)°C to (Tg-100)°C at a rate of 2°C per hour, take it out and cool it naturally. After cutting and polishing, the desired transparent vanadate glass can be obtained. After measurement, its stimulated emission cross section is 4.3pm 2 .

Embodiment 3

[0017] According to the following main substance anion mass percentage V 2 o 5 : 30%; SiO 2 : 20%; Na 2 O: 8%; K 2 O: 12%; Cs 2 O; 3%; CaO: 15%, BaO: 3%, SrO: 9%, Nd 2 o 3 It is 0.5% of the total amount of the former. Weigh the vanadate glass raw material, mix it evenly, add it into a platinum crucible, melt it at 1450°C for 1.5 hours in dry oxygen with a concentration of more than 99%, and cast it into a mold. Cool in the annealing box from (Tg+10)°C to (Tg-100)°C at a rate of 5°C per hour, then take it out and cool it naturally. After cutting and polishing, the desired transparent vanadate glass can be obtained. After measurement, its stimulated emission cross section is 4.6pm 2 .

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Abstract

A series of translucent vanadate glass mixing with Nd3+,V2O5-SiO2-MO(Cao+BaO+SrO)-X2O(Na2O+K2O+Cs2O)-Nd2O3. Compared with previously basic material, the glass has the highest gain parameter and good optical property. They are good candidate material to magnify laser bean and hopeful to make laser system of high-octane nuclear reaction simulation experiment realize physics index, reduce system cost, improve system efficiency.

Description

technical field [0001] The present invention relates to a class of novel laser beam amplification materials (especially fiber laser materials), in particular, the present invention relates to a class of doped rare earth ion Nd 3+ The transparent vanadate glass, which has a high gain coefficient and good optical properties, is expected to achieve its physical indicators, reduce system costs, and improve system efficiency in super-intensive laser systems for high-energy nuclear fusion simulation experiments. technical background [0002] The super-powerful laser system of the high-energy nuclear fusion simulation experiment is not only the hope of new energy for human beings in the future, but also plays an extremely important role in national defense. Especially today when nuclear experiments are completely banned in the world, without the super-powerful laser system of high-energy nuclear fusion simulation experiment, it is impossible to guarantee and continue the national d...

Claims

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Application Information

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IPC IPC(8): C03C3/062
CPCC03C3/062
Inventor 彭波范忠诚仇晓明蒋蕾黄维
Owner FUDAN UNIV
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