Transparent double-sided pressure-sensitive adhesive tape or sheet and touch panel
A technology for contact panels and adhesive tapes, applied in the direction of adhesive types, ester copolymer adhesives, acid copolymer adhesives, etc., can solve the problems of reducing appearance and destroying ornamental properties, and achieve anti-bulging Anti-peeling, anti-warping, and good transparency
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preparation example 1
[0154] [Preparation Example 1 Acrylic polymer]
[0155] Add 97 parts by weight of butyl acrylate as a monomer component, 3 parts by weight of acrylic acid, 0.3 parts by weight of 2,2-azobisisobutyronitrile as a polymerization initiator, and 233.8 parts by weight of ethyl acetate as a polymerization solvent In the detached flask, stirring was carried out for 1 hour while introducing nitrogen gas. In this way, after removing oxygen in the polymerization system, the temperature was raised to 63° C., and the reaction was carried out for 10 hours to obtain an acrylic polymer solution having a solid content concentration of 30% by weight (sometimes referred to as “acrylic polymer solution A”). The weight average molecular weight of the acrylic polymer (it may be called "polymer A") in this acrylic polymer solution A is 550,000.
preparation example 2
[0156] [Preparation Example 2 Acrylic polymer]
[0157] Preparation Example 1 Similarly, an acrylic polymer solution having a solid content concentration of 30% by weight (may be referred to as "acrylic polymer solution B") was prepared. The weight-average molecular weight of the acrylic polymer (may be referred to as "polymer B") in this acrylic polymer solution B is 700,000.
preparation example 3
[0158] [Preparation Example 3 Acrylic polymer]
[0159] Except for using 80 parts by weight of butyl acrylate, 15 parts by weight of methyl acrylate, and 5 parts by weight of acrylic acid as monomer components, an acrylic polymer with a solid content concentration of 30% by weight was obtained in the same manner as in Preparation Example 1 of the acrylic polymer. Polymer Melt (sometimes called "Acrylic Polymer Solution C"). The weight average molecular weight of the acrylic polymer (it may be called "polymer C") in this acrylic polymer solution C is 600,000.
[0160] [Preparation Example 1 Oligomer]
[0161] 96 parts by weight of cyclohexyl methacrylate [the glass transition temperature of the homopolymer (polycyclohexyl methacrylate) is 66°C] as a monomer component, 4 parts by weight of acrylic acid, and 2-mercapto as a chain transfer agent 3 parts by weight of ethanol, 0.2 parts by weight of 2,2'-azobisisobutyronitrile as a polymerization initiator, and 120 parts by weight...
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