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Method for searching analog tobacco leaf based on tobacco leaf near infrared spectra

A technology of near-infrared spectroscopy and search method, which is applied in the direction of material analysis, measuring device, instrument, etc. by optical means, which can solve the problems that the internal quality index cannot find effective components, and the evaluation of the similarity of tobacco leaves is complicated.

Active Publication Date: 2008-08-27
CHINA TOBACCO HUNAN INDAL CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In other industries, such as traditional Chinese medicine, the liquid chromatographic fingerprints of medicinal material extracts have been used for quality determination. However, the internal quality factors of tobacco have a wide range, and many internal quality indicators cannot find the exact corresponding active ingredients. Evaluation of the similarity of tobacco leaves Far more complicated than the quality judgment of traditional Chinese medicine

Method used

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  • Method for searching analog tobacco leaf based on tobacco leaf near infrared spectra
  • Method for searching analog tobacco leaf based on tobacco leaf near infrared spectra
  • Method for searching analog tobacco leaf based on tobacco leaf near infrared spectra

Examples

Experimental program
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Effect test

Embodiment 1

[0044] A total of 2989 samples were taken from 10 to 50 of each of the 115 target tobacco leaves (C1-C115), and the tobacco leaf samples were made by cyclone milling. The near-infrared spectra of all samples were scanned, and the spectral scanning range was 4000 cm. -1 ~10000cm -1 , take the full spectrum area, adopt vector normalization to process the near-infrared spectrum, and establish the data model of 115 target tobacco leaves according to the method of the present invention. In target tobacco leaves C51~C60, respectively get 1 totally 10 independent inspection samples (T51~T60) as unknown tobacco leaves, do the same sample processing and spectral pretreatment as target tobacco leaves, and calculate its difference with target tobacco leaves C1 by the method of the present invention. ~C115 distance, search for the target tobacco leaves most similar to these 10 unknown tobacco leaves. Take the distance calculation between unknown tobacco leaf T51 and target tobacco leaf C...

Embodiment 2

[0073] A total of 2989 samples were taken from 10 to 50 of each of the 115 target tobacco leaves (C1-C115), and the tobacco leaf samples were made by cyclone milling. The near-infrared spectra of all samples were scanned, and the spectral scanning range was 4000 cm. -1 ~10000cm -1 , take the spectral region 4000cm -1 ~7500cm -1 , using mean centering, first-order reciprocal and fitting straight line subtraction to process near-infrared spectra, and establishing data models of 115 target tobacco leaves according to the method of the present invention. In target tobacco leaves C21~C30, get 1 totally 10 independent inspection samples (T21~T30) in addition as unknown tobacco leaves, do the same sample processing and spectral pretreatment as target tobacco leaves, search for these 10 unknown by the method of the present invention The tobacco leaf most similar to the target tobacco leaf. Table 2 lists the top 7 target tobacco leaves that are most similar to the 10 unknown tobacco...

Embodiment 3

[0078] A total of 2,989 samples were taken from 10 to 50 of each of the 115 target tobacco leaves (C1 to C115), cut into shreds to make shredded tobacco samples, and scanned the near-infrared spectra of all samples, with a spectral scanning range of 4,000 cm -1 ~10000cm -1 , take the spectral region 5200cm -1 ~6800cm -1 、7500cm -1 ~9000cm -1 , using mean centralization and second-order reciprocal to process near-infrared spectra, and establishing data models of 115 target tobacco leaves according to the method of the present invention. In the target tobacco leaves C71~C80, get 1 total 10 independent inspection samples (T71~T80) in addition as unknown tobacco leaves, do the same sample processing and spectral pretreatment as the target tobacco leaves, and search for these 10 unknown samples by the method of the present invention. The tobacco leaf most similar to the target tobacco leaf. Table 3 lists the top 7 target tobacco leaves that are most similar to the 10 unknown t...

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Abstract

The present invention relates to a similar tobacco leaves search method based on the near infrared spectrum of tobacco leaves. The near infrared spectrum of tobacco leaves is used as basic data by the present invention. Distributed sampling is first carried out to the target tobacco leaves of each species; samples are pre-treated; the near infrared spectrum of the samples is obtained by scanning the samples on a near infrared spectrometer; principal component analysis (PCA) operation is carried out to a plurality of near infrared spectra of the target tobacco leaves of each species, obtaining loading matrixes, characteristic values and standardized residual errors, so as to generate a data model of the target tobacco leaves of each species; the near infrared spectrum of an unknown tobacco leaf, and the loading matrixes in the target tobacco leaf data models are used to carry out principal component decomposition calculation to the near infrared spectrum of the unknown tobacco leaf, so as to obtain the principal component score and decomposition residual error of the unknown tobacco leaf; the principal component score of the unknown tobacco leaf and the principal component space distance of the target tobacco leaf data models are calculated, and the residual error distance between the decomposition residual error of the unknown tobacco leaf and the standardized residual errors in the target tobacco leaf data models is also calculated; the distance between the unknown tobacco leaf and the target tobacco leaves is measured through the sum square root of the principal component space distance and the residual errors; the smaller the distance is, the higher the similarity is; finally, the distances between the unknown tobacco leaf and each target tobacco leaf is compared and sorted according to the size of the distances, so as to obtain a similar tobacco leaves search result.

Description

technical field [0001] The invention relates to a method for searching similar tobacco leaves in the tobacco industry. The search result is obtained by calculating the similarity between unknown tobacco leaves and various target tobacco leaves. Background technique [0002] The internal quality of tobacco leaves is affected by factors such as climatic conditions, planting regions, planting management, and processing. Tobacco leaf raw materials of various origins and varieties are mainly classified into different grades according to their appearance quality, and the correspondence between the appearance quality and internal quality of tobacco leaves is not exact. Therefore, before the tobacco raw materials are used in formula design and industrial production by tobacco processing enterprises, they need to be manually evaluated to determine their inherent quality characteristics. The sources of tobacco leaves involved in product design are complicated, and there are hundreds o...

Claims

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Application Information

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IPC IPC(8): G01N21/17G06F17/10
Inventor 杜文易建华谭新良任建新张文利周燕
Owner CHINA TOBACCO HUNAN INDAL CORP
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