Polymeric MEA for fuel cell
A polyelectrolyte and mixture technology, applied in fuel cells, fuel cell components, solid electrolyte fuel cells, etc., can solve problems such as unsatisfactory dimensional stability, low proton conductivity, low membrane/electrode interface stability, etc.
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Embodiment 1
[0146] Example 1: Preparation of polyelectrolyte membrane comprising sulfonated polysulfone ketone copolymer
[0147] Synthesis of Sulfonated Polysulfone Ketone Copolymer
[0148] In a 100 ml 3-bulb flask equipped with a Dean-Stark trap and condenser, 0.01 mole of bisphenol A, 0.005 mole of 4,4'-difluorobenzophenone and 0.005 mole of 3 , 3'-disodiumsulfonyl-4,4'-difluorophenylsulfone was dissolved in 15 ml of N-methylpyrrolidone (NMP). Subsequently, 0.00002 mol of tris-4-hydroxyphenylethane (0.2 mol% based on bisphenol A) was added.
[0149] Join K 2 CO 3 (0.026 mol), heated to 70° C., and 10 ml of toluene was added, reflux reaction was carried out for 5 hours, and the generated water was removed.
[0150] After removing water, heat to 160°C to remove toluene. Subsequently, the reaction was further performed at 160° C. for about 6 hours to prepare a sulfonated polysulfoneketone copolymer.
[0151] The sulfonated polysulfoneketone copolymer thus prepared was precipita...
Embodiment 2
[0154] Example 2: Preparation of Polyelectrolyte Membrane Comprising 1% by Weight PVDF
[0155] A hybrid membrane was prepared in the same manner as in Example 1, except that 1% by weight of PVDF based on the sulfonated polysulfoneketone copolymer was introduced.
Embodiment 3
[0156] Example 3: Preparation of a polyelectrolyte membrane comprising 1.5% by weight PVDF
[0157] A hybrid membrane was prepared in the same manner as in Example 1, except that 1.5% by weight of PVDF based on the sulfonated polysulfoneketone copolymer was introduced.
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Abstract
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