Medium temperature iron-manganese desulfurizing agent and preparation method thereof
A desulfurizer, iron and manganese technology, applied in separation methods, chemical instruments and methods, dispersed particle separation, etc., can solve the problems of inability to fundamentally improve the penetrating sulfur capacity of iron and manganese desulfurizers, unsatisfactory desulfurization effect, etc. The best desulfurization effect, the guarantee of mechanical strength, the effect of high penetration sulfur capacity
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[0023] Example 1
[0024] Take 85g Fe 3 O 4 , 10g MnO 2 , 5g bentonite, mix the above-mentioned substances well, then add an appropriate amount of water to the above-mentioned mixture, stir the above-mentioned substances thoroughly, knead them, and then carry out extrusion molding.
[0025] The above-mentioned molded product was calcined at 300 ° C for 4.5 hours. 3 O 4 and MnO 2 Evenly distributed on it, together constitute the iron-manganese desulfurizer A of the present invention, and the iron oxide Fe in the desulfurizer is 3 O 4 The content is 85 wt %, the manganese oxide content is 10 wt %, and the inorganic binder content is 5 wt %.
Example Embodiment
[0026] Example 2
[0027] Take 77.9g iron oxyhydroxide FeOOH, 28.4g manganese carbonate MnCO 3 , 5g sheep liver soil and 5g cement, mix the above-mentioned substances fully, then add an appropriate amount of water to the above-mentioned mixture, fully stir the above-mentioned substances, knead and extrude them.
[0028] The above-mentioned molded product is placed in the environment of 350 ° C and calcined for 5 hours. After calcination, FeOOH in the raw material is converted into Fe. 2 O 3 , MnCO3 Conversion to MnO and MnO 2 , the calcination of sheep liver soil and cement makes its structure as a support carrier more dense, and the resulting Fe 2 O 3 and MnO 2 Evenly distributed on it, together constitute the iron-manganese desulfurizer B of the present invention, and the iron oxide Fe in the desulfurizer is 2 O 3 The content is about 70 wt %, the manganese oxide content is about 20 wt %, and the inorganic binder content is 10 wt %.
Example Embodiment
[0029] Example 3
[0030] Take 50g Fe 2 O 3 , 49g MnCO 3 , 15g attapulgite, mix the above-mentioned substances well, then add an appropriate amount of water to the above-mentioned mixture, fully stir the above-mentioned substances, knead them and then carry out extrusion molding.
[0031] The above-mentioned molded product was calcined at 400 ° C for 4 hours. After calcination, the MnCO in the raw material was calcined. 3 Conversion to MnO and MnO 2 , the structure of attapulgite as a support carrier becomes denser after calcination, Fe 2 O 3 , MnO and MnO 2 Evenly distributed on it, together constitute the iron-manganese desulfurizer C of the present invention, and the iron oxide Fe in the desulfurizer is 2 O 3 The content is about 50wt%, the manganese oxide content is 35wt%, and the inorganic binder content is 15wt%.
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