Device and method for detecting molecular interactions
A technology of target molecules and probe molecules, which is applied in the field of specific interaction devices, can solve the problems of reducing the detection signal, slowing down the detection method, etc., and achieves the effects of improving repeatability, avoiding pollution, and facilitating external intervention.
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Embodiment 1
[0323] Example 1: Structure of a reaction chamber with an integrated heater
[0324] exist Figure 8 and Figure 9 An embodiment of a processing unit without an integrated heater and a device for directing a DNA chip towards a detection plane is described in . The DNA chip in the shown device can be read out by a conventional fluorescence microscope (eg Axioskop, Zeiss, Jena, Germany).
Embodiment 2
[0325] Example 2: Structure of a reaction chamber with a silicon heating substrate
[0326] Figure 10 and 11 The variant of the processing unit of the device of the invention shown in is a miniaturized reaction chamber containing an integrated probe array (DNA chip), a silicon heating substrate with integrated temperature sensors for regulating the different temperatures in the reaction chamber ("heating substrate"), and optionally a circuit board with EPROM for making electrical contact with the heating substrate. Each element is embedded in two shells made of synthetic material. The entire unit is a spatially closed system in which all required reactions (eg PCR) can be performed in a temperature-controlled manner.
[0327] First insert the board into the posts provided in the lower case (with the EPROM facing down). On the upper side of the circuit board, three electrical contact pads are arranged, which ensure the electrical connection to the subsequently inserted h...
Embodiment 3
[0334] Example 3: Detection of background signal reduction by dislocation of analyte
[0335] All fluorescence measurements described in this example were performed by a fluorescence microscope (Zeiss, Jena, Germany). Excitation was performed with incident light using a white light source, and filters were set to suit cyanine 3. Signals were recorded by a CCD camera (PCO-Sensicam, Kehlheim, Germany). In the underside, the thickness of the slit represents the distance between the microarray and the detection plane.
[0336] a) Measure the fluorescence signal of the analyte according to the thickness of the slit
[0337] Channel shells with defined channel depths (5m, 10m, 28m) were cast by Sylgard. The width of the channel is 125 μm. Glass chips are placed in channels of varying depths. The channel was then filled with a solution of 200 nM Cy-3 labeled oligonucleotide in 2x SSC + 0.2% SDS and the signal was measured using an exposure time of 1.5 seconds.
[0338] exist ...
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Abstract
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