Semen Cassiae Composite Antibacterial Finishing Agent, Preparation Method, Fiber Treatment Method and Application
A technology of compounding antibacterial and finishing agents, which is applied in application, fiber treatment, household appliances, etc., to achieve the effect of convenient use, high efficiency and long-lasting antibacterial effect, and excellent washing resistance.
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Embodiment 1
[0032] Preparation of Semen Cassiae Extract: Purify and pulverize Semen Cassiae, add ethyl acetate, and extract by heating and reflux or cold soaking. 20-90 minutes each time; or cold extraction 1-5 times, 9-24 hours each time; the extracts were combined; the extracts were filtered and the solvent was recovered to obtain the cassia seed ethyl acetate extract. The cassia seed extract contains the following active ingredients: active ingredients of anthraquinones ≥ 0.1 parts by weight, active ingredients of piroxins ≥ 0.165 parts by weight, and active ingredients of polysaccharides ≥ 20.8 parts by weight.
Embodiment 2
[0034] Preparation of nano cassia seeds: After drying cassia seeds at low temperature, they are routinely crushed into 80-200 mesh fine powder, and then the fine powder is put into the crushing cylinder of a fully enclosed centrifugal shear ultrafine pulverizer with a jacket for continuous crushing. The temperature is controlled at room temperature, the spindle speed is 800-2400rpm, and the pulverization time is 30-90 minutes, and pulverized into a homogeneous superfine powder with a particle size of 50-200nm. The nano cassia seed contains the following active ingredients: active ingredients of anthraquinones ≥ 0.1 parts by weight, active ingredients of piroxins ≥ 0.165 parts by weight, and active ingredients of polysaccharides ≥ 20.8 parts by weight.
Embodiment 3
[0036] Preparation of nano cassia seeds: add distilled water as a dispersant to the coarsely processed cassia seeds fine powder, the weight ratio of cassia seeds fine powder to distilled water is 1:20-30, after the dispersion is even, soak for 1-24 hours, and then the fine powder Put it into the pulverizing barrel of a fully enclosed centrifugal shear ultrafine pulverizer with a jacket for continuous pulverization, the working temperature is controlled at room temperature, the spindle speed is 800-2400rpm, the pulverization time is 30-90 minutes, and the pulverization into a particle size of 50-200nm homogeneous ultrafine powder. The nano cassia seed contains the following active ingredients: active ingredients of anthraquinones ≥ 0.1 parts by weight, active ingredients of piroxins ≥ 0.165 parts by weight, and active ingredients of polysaccharides ≥ 20.8 parts by weight.
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