Manufacturing method of high-purity nickel strap

A manufacturing method and technology for nickel strips, applied in manufacturing tools, metal rolling, welding equipment, etc., can solve the problems of inability to adopt, high price of nickel plates, loss of various components of rolling mills, etc., to solve the serious decline in purity and reduce nickel Process loss, low loss of rolling mill components

Active Publication Date: 2012-09-19
YULIN NORMAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These nickel plates are more expensive
And since electrolytic nickel plates are mostly used in the electroplating industry or cut into small pieces of nickel for smelting and adding alloying elements (such as stainless steel), whether there is obvious delamination and / or micropores in the electrolytic plate will not have a negative impact on these applications , so most electrolytic nickel plate production plants do not need or take the initiative to increase equipment and production input to reduce delamination and / or porosity defects inside the electrolytic nickel plate
[0008] 2. Low production efficiency, high energy consumption and serious loss of parts of the rolling mill due to the use of cold rolling billets
[0010] 3. With the conventional welding method, the purity near the joint is low, and the thickness fluctuates greatly, which will affect the consistency of the high-purity nickel strip
[0013] 1. Using cold rolling to open the billet, the production efficiency is low, the energy consumption is high and the parts of the rolling mill are seriously worn out
Moreover, for electrolytic nickel sheets with delamination and / or microporous defects inside, cold rolling with a small amount of deformation first will generate a large shear force near the internal defects, which will easily lead to accelerated propagation of crack defects in the material until delamination failure
[0014] 2. The vacuum heat treatment furnace with intermittent operation used many times in its process will seriously affect the output of high-purity nickel strips mainly thin strips
[0015] 3. After several cold rolling processes, the electrolytic nickel plate will be extended to more than several meters along the length direction (the raw material electrolytic nickel plate is generally about 1 meter long) and cannot be coiled, but it can be heat-treated at such a shape and length at high temperature Due to the high cost of vacuum heat treatment furnace, it is actually impossible to adopt it in production practice.
[0016] The above-mentioned prior art is still unable to be applied and promoted on a large scale due to the relatively large defects in the mass production practice of high-purity nickel strips.

Method used

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  • Manufacturing method of high-purity nickel strap
  • Manufacturing method of high-purity nickel strap
  • Manufacturing method of high-purity nickel strap

Examples

Experimental program
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Effect test

Embodiment 1

[0054] Example 1: A soft high-purity nickel strip with a thickness of 0.2 mm and a width of 100 mm was prepared. The raw material is 10 electrolytic nickel plates, the basic size: thickness 15mm x width 600mm x length 1200mm, composition: Ni weight percentage ≥ 99.97%.

[0055] see figure 1 , the method that embodiment 1 manufactures high-purity nickel strip may further comprise the steps:

[0056] (1) Ultrasonic flaw detection and sorting. Fully automatic ultrasonic non-destructive testing was carried out on 10 incoming electrolytic nickel plates, and it was found that 5 of the plates had only delamination defects and no other defects inside, and 2 plates had both delamination defects and micropore defects (the diameter of the micropores was basically at 1mm), 3 boards have no delamination and micropore defects, that is, after sorting, 7 electrolytic nickel boards are found to have delamination defects, and 3 boards have no internal defects.

[0057] ⑵ Carry out correspond...

Embodiment 2

[0063]Embodiment 2: Prepare a 1 / 2 hard high-purity nickel strip with a thickness of 0.15 mm and a width of 19 mm. The raw material is 10 electrolytic nickel plates, the basic size: thickness 15mm x width 600mm x length 1200mm, composition: Ni weight percentage ≥ 99.97%.

[0064] refer to figure 2 , the method that embodiment 2 manufactures high-purity nickel strip may further comprise the steps:

[0065] (1) The whole electrolytic nickel plate is hot-rolled and billeted. The entire electrolytic nickel plate is placed in a chain-type continuous heating furnace in sequence, and a protective atmosphere (ammonia decomposition gas) is introduced into the furnace. The heating temperature is 1050 ° C, and the entire heating time is 15 minutes. It is rolled immediately after being released from the furnace. Each nickel plate is hot-rolled 5 times, from 15mm to 2.5mm thick, wherein the deformation rate of the first pass is 35%, and the rolling deformation rate of the other passes is...

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Abstract

The invention discloses a manufacturing method of a high-purity nickel strap. The method comprises the steps of hot rolling and cogging an un-smelted nickel plate, then processing the cogged semi-finished product into a nickel strap with desired thickness through at least one annealing process and at least one cold rolling process. According to the manufacturing method, not only can the high purity of the material be guaranteed, the energy consumption and the nickel loss are reduced, the delamination defect in an electrolytic nickel raw material plate can be repaired effectively; the pass percent is high by adopting the electrolytic nickel raw material plate provided by a plurality of existing electrolytic nickel plate manufacturers, and the produced nickel strap has good consistency; and meanwhile, due to the method, the production efficiency is high, the energy consumption is low, and rolling mill component loss is small.

Description

technical field [0001] The invention relates to a method for manufacturing a high-purity nickel strip, more specifically a method for directly using an electrolytic nickel plate to manufacture a high-purity nickel strip. Background technique [0002] High-purity nickel strips generally refer to nickel strips containing more than 99.9% by weight of Ni. Compared with the currently commonly used Ni200 and Ni201 strips (containing less than 99.8% by weight of Ni), the higher purity of nickel will bring characteristics that conventional pure nickel materials cannot possess, such as high-purity nickel with higher conductivity, Better flexibility, lower recrystallization temperature. The market and application of high-purity nickel are very extensive. Among them, the high-purity nickel plate can be directly used as an additive element in the development of superalloys and new alloys in the aviation and cosmic atomic industries, for the processing of high-tension alloy parts in ae...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B23P17/04B23P25/00B23K31/02B21B3/00C22F1/10
Inventor 沈翠珊
Owner YULIN NORMAL UNIVERSITY
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