Small multifunctional sample room for LIBS (laser-induced breakdown spectroscopy)

A technology of laser-induced breakdown and sample chamber, which is applied in the direction of material excitation analysis, material analysis through optical means, and measurement equipment, etc., can solve the problem that is contrary to the original intention of LIBS in-situ analysis, the analysis results are not representative, and the sample cannot be directly analyzed. Measurement and other issues, to achieve the effect of good work reliability, good focus, and good sealing

Active Publication Date: 2012-09-26
SICHUAN UNIV
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AI Technical Summary

Problems solved by technology

[0004] The sample chamber is a very important part of the LIBS system. At present, in the application process of LIBS technology, the sample chamber is mostly set based on a single mobile platform, which can only realize small-scale movement mainly based on two-dimensional or three-dimensional translation.
The open sample platform is mostly used on the LIBS platform built by the laboratory. Although the sample chamber in the commercial LIBS instrument is made into a closed type after appropriate modification, it can only carry one sample at a time for LIBS measurement, and the powder sample Most of the analysis requires pre-processing such as briquetting, which is contrary to the original intention of using LIBS in situ an

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  • Small multifunctional sample room for LIBS (laser-induced breakdown spectroscopy)
  • Small multifunctional sample room for LIBS (laser-induced breakdown spectroscopy)
  • Small multifunctional sample room for LIBS (laser-induced breakdown spectroscopy)

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Example Embodiment

[0022] Example 1

[0023] The multifunctional sample chamber of this embodiment that can be used for laser-induced breakdown spectroscopy analysis has a structure as attached figure 1 And figure 2 As shown, a closed chamber 7 that can be opened from the top of the chamber shell, a quartz focusing lens 1 arranged on the top of the chamber shell, a sample tray 3 installed on a rotatable lifting column 8 located in the center of the chamber bottom, and A signal collection device 9 connected to an external detector on the wall of the chamber is composed of. The sample plate and the plate of the rotating lifting column platform 8 are fixedly arranged together by a buckle, and the rotating lifting column platform is driven to move by a stepping motor. The sample tray is designed with 8 symmetrically arranged circular pit sample cells 2, which are located on the same diameter circle in the surface of the sample tray. When the sample tray rotates, it can be turned directly below the qu...

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Abstract

The invention discloses a small multifunctional sample room for LIBS (laser-induced breakdown spectroscopy), whose structure mainly includes an openable closed cavity, a focusing lens arranged on a casing top of the cavity, a sample plate mounted on a rotatable lifting column table positioned at the center of the bottom of the cavity, and a signal collection device placed on the casing wall of the cavity and connected with an external detector, wherein no less than one sample cell is designed on the sample plate, is positioned in the sample plate and can rotate to the position below the focusing lens during the rotation of the sample plate; and a lens of the signal collection device points to the sample cell rotating to the position below the focusing lens. The small multifunctional sample room disclosed by the invention can be used for bearing solid particulates, powders and liquid samples simultaneously for measurement, has the characteristics of excellent focusing performance, tightness and working performance, small volume and the like, can be integrated in a laser optical spectrum analyzer or used independently, and is particularly suitable for simultaneously analyzing in-situ collected scraps, rock and slurry samples in petroleum drilling and geological exploration.

Description

technical field [0001] The invention relates to a laser-induced breakdown spectrum sample detection technology, in particular to a small multifunctional sample chamber which can be used for laser-induced breakdown spectrum analysis. Background technique [0002] In the oil exploration industry, through the analysis of the components of drilling fluid, rock and mud on site, it provides a basis for exploration and development decisions, which is an important method to improve the compliance rate of mud logging interpretation and effectively exploit oil and mineral resources. Introduce real-time in-situ testing technology suitable for simultaneous analysis of multi-components and multi-forms to realize real-time analysis of on-site samples and quickly obtain comprehensive first-hand collection data, so as to make correct mud logging interpretation and evaluation, and improve oil and mineral production. The development efficiency of resources can promote the progress of the indu...

Claims

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Application Information

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IPC IPC(8): G01N21/63
CPCG01N21/718
Inventor 段忆翔林庆宇刘安良何毅杨光
Owner SICHUAN UNIV
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