Activated peroxide cleaning compositions
A technology of cleaning composition and peroxygen compound, which is applied in the field of metallocarbene complexes and cleaning compositions containing bleach, and can solve problems such as poor fabric safety, poor solubility, and poor bleaching
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example 1
[0056] The following procedure was used to assess the relative reactivity of different potential catalytic activators with hydrogen peroxide: 10 mg of activator was filled into a 20-ml glass scintillation vial. Aqueous hydrogen peroxide (5 ml of 5% hydrogen peroxide solution) was charged to individual vials and the vials were vortexed slowly to provide mixing. The degree of bubbling and gas evolution was rated visually for approximately the first 10 minutes after the addition of hydrogen peroxide and was classified using the following scale (1-6), where lower numbers indicate greater reactivity: 1 = very intense ; 2=strong; 3=moderate; 4=little; 5=very slight; 6=none. Table 5 summarizes the results.
[0057] table 5
[0058] example
[0059] 2
[0060] These M-carbene-containing activators exhibited the highest reactivity with hydrogen peroxide. M-carbene activators 1, 2, and 6 all showed higher reactivity than the three comparative activators (TAED, A35...
example 2
[0061] Example 2: Cleaning experiment
[0062] Tables 6 and 7 show the composition of Test Formulations A-R, which were used in Evaluations 1-96; unless otherwise noted, entries reflect the mass (mg) of the different ingredients used in the 1-L reactor beaker. Load metal containing activators to provide cleaning approx. 1.1x10 -5 The in-wash metal concentration in mol / L. The A350 entry represents the Mn-containing activator tris-mu-oxo-bis[(1,4,7-trimethyl-1,4,7- The mass of triazacyclononane) manganese] bis(acetate). when in When the specific concentration of Mn in the TRS KB2 formulation was not readily available, KB2 was loaded according to the manufacturer's recommendations (approximately 0.5%-2.0%). Take about 1.1 x 10 -5 mol / L to use the organic activator TAED.
[0063] Table 6
[0064]
[0065]
[0066] *A350 entry represents the Mn-containing activator tris-mu-oxo-bis[(1,4,7-trimethyl-1,4,7 - mass of triazacyclononane) manganese]bis(acetate).
[0067]...
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