Method for preparing magnetic SBA-15
A SBA-15, magnetic technology, applied in chemical instruments and methods, molecular sieve compounds, inorganic chemistry, etc., can solve the problems of high synthesis cost of instruments and equipment, and achieve the effect of low production cost, high porosity, and large specific surface area
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[0019] First weigh 1.5g of ferrous chloride, stir it in the dark, dissolve it in a beaker with 50ml of deionized water, then add 2g of P123 to the beaker, stir magnetically at room temperature to form a uniform solution, then add 4.25 g TEOS, stirred at 40°C for 20h, then transferred the reaction product and mother liquor to a polytetrafluoroethylene stainless steel hydrothermal kettle, and heated it at 100°C for 72h, after cooling, the sample was filtered, oven-dried, and finally in air atmosphere Calcined at 500°C for 6 hours to remove the template and obtain a magnetic SBA-15 sample with a specific surface area of 749m 2 / g, pore diameter 7.5nm, pore volume 1.40cc / g.
[0020] The scanning electron microscope picture of the magnetic SBA-15 mesoporous molecular sieve material prepared in this embodiment is as follows figure 1 shown.
[0021] The transmission electron microscope picture of the magnetic SBA-15 mesoporous molecular sieve material prepared in this embodiment ...
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