Preparation method of super-hydrophobic-hydrophilic wood with intelligent temperature response

A temperature-responsive, super-hydrophobic technology, applied in wood impregnation, wood treatment, impregnated wood, etc., can solve problems such as the inability to meet the needs of daily life, single super-hydrophobic performance of super-hydrophobic wood, and achieve low cost, short cycle, The effect of avoiding research investment

Inactive Publication Date: 2015-07-29
GUANGDONG YIHUA TIMBER IND
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Problems solved by technology

The existing superhydrophobic wood preparation method is generally to add inorganic particles to the wood, followed by beeswax treatment, etc. The prepared superhydrophobic wood only has a single superhydrophobic property, which cannot meet the needs of daily life. Therefore, how to improve the superhydrophobic wood? The intelligent responsiveness of hydrophobic wood has become a research hotspot for current researchers

Method used

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  • Preparation method of super-hydrophobic-hydrophilic wood with intelligent temperature response
  • Preparation method of super-hydrophobic-hydrophilic wood with intelligent temperature response
  • Preparation method of super-hydrophobic-hydrophilic wood with intelligent temperature response

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specific Embodiment approach 1

[0018] Specific embodiment one: the preparation method of intelligent temperature-responsive super-hydrophobic-hydrophilic wood in this embodiment is carried out according to the following steps:

[0019] Step 1, the wood is ultrasonically cleaned with deionized water, acetone and absolute ethanol in sequence, and dried at 60°C for 12h to 24h;

[0020] Step 2. Weigh 0.2g of silicon dioxide with a particle size of 250nm and disperse it in 100mL of deionized water. Ultrasonic disperse for 0.5h at a working frequency of 50KHz, a power of 100%, and a temperature of 25°C, and then soak the wood in it 24h, then placed in a drying oven at 60°C for 24h;

[0021] dispersion

[0022] Step 3, prepare a mixed solution with methanol and chloroform at a volume ratio of 1:3, dissolve 0.025g of polycaprolactone in 5ml of the mixed solution, and then evenly drop-coat it on the horizontal surface of the wood treated in step 2 Place the cut surface in a vacuum drying oven, vacuumize to -0.8kPa...

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Abstract

The invention relates to a preparation method of super-hydrophobic-hydrophilic wood with intelligent temperature response and belongs to the field of super-hydrophobic wood. The super-hydrophobic wood prepared by the method has the hydrophilic reversible characteristic which is not owned by the previous super-hydrophilic wood. A contact angle between the super-hydrophobic wood and water is greater than 150 degrees; a rolling angle is smaller than 10 degrees; the super-hydrophobic-hydrophilic wood is excellent in super-hydrophobic performance and good in self-cleaning performance. The preparation method of the super-hydrophobic-hydrophilic wood with the intelligent temperature response comprises the following steps: soaking the wood in a silicon dioxide aqueous solution, drying, then uniformly and dropwise coating the surface of the wood with polycaprolactone dissolved in a mixed solution of methyl alcohol and chloroform, and finally drying in vacuum. The wood shows the intelligent temperature response in the cross section. The method is simple in process, low in cost, short in period, low in energy consumption and free of special complicated equipment; the prepared super-hydrophobic-hydrophilic wood with the intelligent temperature response is capable of converting the wettability for hundreds of times under high and low temperatures; the prepared super-hydrophobic-hydrophilic wood has a great application prospect in the future.

Description

technical field [0001] The invention belongs to the technical field of wood; in particular, it relates to a preparation method of intelligent temperature-responsive superhydrophobic-hydrophilic wood. Background technique [0002] Wood is a traditional material that plays an extremely important role in production and life. For example, in the construction industry, wood, as an excellent natural material, has an indispensable position in ancient Chinese palace buildings; in the furniture industry, wood, as a non-toxic and harmless material with natural texture, often appears in some high-end furniture supplies. However, due to the obvious hygroscopic phenomenon of traditional wood, if it is placed in an environment with high humidity for a long time, mildew and corrosion will occur. At the same time, its dimensional stability cannot be guaranteed, which greatly reduces the durability of wood. service life. Therefore, the research on wood with superhydrophobic properties is ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B27K3/02B27K3/50
CPCB27K3/02B27K3/50B27K2240/70
Inventor 王成毓高正鑫
Owner GUANGDONG YIHUA TIMBER IND
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