Efficient agricultural herbicide
A herbicide and agricultural technology, applied in the agricultural field, can solve the problems of unpredictable weeding effect, conflict of chemical components, reduction of wheat yield, etc.
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Embodiment 1
[0017] Example 1: Compound (I) Separation Preparation and Structure Confirmation
[0018] Sources of reagents: ethanol, petroleum ether, ethyl acetate, n-butanol, and dichloromethane were of analytical grade, purchased from Shanghai Lingfeng Chemical Reagent Co., Ltd. Methanol, of analytical grade, were purchased from Jiangsu Hanbang Chemical Reagent Co., Ltd.
[0019] Preparation method: (a) Grind the dried and mature seeds (1kg) of wangbuliuxing, extract with 85% ethanol under hot reflux, combine the extracts, concentrate until there is no alcohol smell, and successively add petroleum ether, ethyl acetate and water-saturated n-butanol extraction to obtain petroleum ether extract, ethyl acetate extract and n-butanol extract respectively; % ethanol for 6 column volumes, then 75% ethanol for 10 column volumes, collect the 75% ethanol eluate, concentrate under reduced pressure to obtain the 75% ethanol eluate extract; (c) in step (b) The 75% ethanol eluted extract was separated...
Embodiment 2
[0022] Embodiment 2: preparation and herbicidal effect of herbicide
[0023]Take an appropriate amount of solvent DMSO to dissolve isoproturon and compound (I), then dilute with tap water, the molar concentration of isoproturon is 80 μg / ml, and the molar concentration of compound (I) is 320 μg / ml. The molar concentration of the compound (I) is 3 to 5 times that of the isoproturone.
[0024] How to use: Spray twice a week.
[0025] To investigate index to the inhibition rate of wheat field sage, japonica, chickweed, cow chickweed, test group one and test group two are set respectively, test group one sprays the herbicide provided by the present invention, and test group two weed control The dose contained only isoproturon at the same concentration as the test group one. The trial period is 1 month. The results are shown in the table below.
[0026]
[0027] The results show that in the herbicide of the present invention, compound (I) has played a very important ro...
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