Novel environment-friendly modified bentonite PVC heat stabilizer
A technology of heat stabilizer and bentonite, which is applied in the field of new environment-friendly modified bentonite PVC heat stabilizer, can solve the problems of unstable quality, low alkali capacity of alkaline clay, poor lipophilicity, etc. Shortening and good compatibility
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[0037] A kind of novel environmental protection modified bentonite PVC heat stabilizer, its preparation method comprises the following steps:
[0038] S1: Mix bentonite and activated clay wastewater with a concentration of 10%-16% in a weight ratio of 1.6-2.2:10-14, and stir evenly at a rotating speed of 200-500r / min to obtain a slurry material A;
[0039] S2: Add the slurry material A prepared in step S1 to the inorganic mixed acid with a concentration of 11%-20%, the inorganic mixed acid is carbonic acid with a concentration of 22-26wt%, oxalic acid with a concentration of 28-32wt%, and 18-20wt% phosphoric acid is a mixed acid composed of a volume ratio of 3-5:2-4:2-3, the weight ratio of the slurry material A to the inorganic mixed acid is 1-3.2:4-16, and the rotating speed is 200- Add sodium trisulfide and stir at 550r / min, the weight ratio of sodium trisulfide to slurry material A is 1-2:50-150, heat to 82-93°C, keep at 82-93°C for 1.2-3.2h, Obtain slurry material B;
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Embodiment 1
[0050] A kind of novel environmental protection modified bentonite PVC heat stabilizer, its preparation method comprises the following steps:
[0051] S1: Mix bentonite and activated clay wastewater with a concentration of 12% at a weight ratio of 2:12, and stir evenly at a rotation speed of 400r / min to obtain slurry material A;
[0052] S2: Add the slurry material A prepared in step S1 into the inorganic mixed acid with a concentration of 15%, the inorganic mixed acid is carbonic acid with a concentration of 22wt%, oxalic acid with a concentration of 28wt%, and phosphoric acid with a concentration of 18wt% by volume Mixed acid composed of 3:2:2, the weight ratio of slurry material A to inorganic mixed acid is 2:10, add sodium trisulfide and stir at a speed of 400r / min, the weight ratio of sodium trisulfide to slurry material A 2:120, heated to 85°C, kept at 85°C for 2.5h to prepare slurry material B;
[0053] S3: press-filter the slurry material B prepared in step S2 at a pr...
Embodiment 2
[0062] A kind of novel environmental protection modified bentonite PVC heat stabilizer, its preparation method comprises the following steps:
[0063] S1: Mix bentonite and activated clay wastewater with a concentration of 16% at a weight ratio of 2.2:14, and stir evenly at a speed of 500r / min to obtain a slurry material A;
[0064] S2: Add the slurry material A prepared in step S1 into the inorganic mixed acid with a concentration of 20%, the inorganic mixed acid is carbonic acid with a concentration of 26wt%, oxalic acid with a concentration of 32wt%, and phosphoric acid with a concentration of 20wt% by volume Mixed acid composed of 5:4:3, the weight ratio of slurry material A to inorganic mixed acid is 3.2:16, add sodium trisulfide and stir at a speed of 550r / min, the weight ratio of sodium trisulfide to slurry material A 2:150, heated to 93°C, kept at 93°C for 1.2h to prepare slurry material B;
[0065] S3: press-filter the slurry material B prepared in step S2 at a press...
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