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Quality detection method of rejuvenating and life prolonging paste

A quality inspection method, the technology of Schisandra chinensis, applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of no identification method, great influence on the quality of Changchun Yishou ointment, and affect the curative effect of the product, so as to achieve high-quality standards and improve The effect of simple quality control standards and quality inspection methods

Inactive Publication Date: 2016-12-14
JIANGSU 707 NATURAL PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The two have a greater impact on the quality of Changchun Yishou Gao
[0013] However, the existing quality standards only have traits and inspection items, and there is no identification method, so the product quality cannot be well controlled, thus affecting the curative effect of the product

Method used

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  • Quality detection method of rejuvenating and life prolonging paste
  • Quality detection method of rejuvenating and life prolonging paste

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] Changchun Yishou Gao was prepared according to the formula and method in the drug standard issued by the Ministry of Health (the 19th volume of traditional Chinese medicine preparations).

Embodiment 2

[0040] Embodiment 2: the TLC identification of Schisandra chinensis

[0041] Preparation of the test solution: Take 20 g of this product, add 50 mL of chloroform, ultrasonically extract for 30 minutes, evaporate the chloroform to dryness, add 1 mL of chloroform to the residue to dissolve as the test solution.

[0042] Preparation of the reference medicinal material solution: Take another 1 g of Schisandra chinensis, add 25 mL of chloroform, ultrasonically extract for 30 minutes, evaporate the chloroform solution to dryness, add 1 mL of chloroform to dissolve the residue, and use it as the reference medicinal material solution.

[0043] Preparation of negative reference solution: take the negative sample lacking Schisandra chinensis, and use the same method as the test solution to prepare a negative reference solution.

[0044] Thin-layer chromatography: draw 10 μL of each of the above three solutions, spot on the same silica gel G thin-layer plate, use petroleum ether (30-60 °...

Embodiment 3

[0046] Embodiment 3: the TLC identification of Asparagus

[0047] Preparation of the test solution: Take 40 g of Changchun Yishou Gao, add 5 ml of hydrochloric acid and 50 ml of distilled water, hydrolyze for 2 hours under reflux in a water bath, place at room temperature, filter, wash the filter residue with a small amount of water, dry it in an oven, add ethyl acetate 10 ml, sonicated for 10 min, filtered, and the filtrate was concentrated to 1 ml as the test solution.

[0048] Preparation of the reference medicinal material solution: take 2 g of Asparagus medicinal material, and the method is the same as above. As a reference medicinal solution.

[0049] Preparation of negative control solution: Take 2 times the amount of asparagus, take other medicinal materials except asparagus, and extract with water, the method is the same as above. as a negative control solution.

[0050] Thin-layer chromatography: Take 5 μL of each sample solution for spotting, respectively spot on...

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Abstract

The invention discloses a quality detection method of rejuvenating and life prolonging paste. The quality detection method comprises the steps of ingredient identification on fructus schisandrae and ingredient identification on radix asparagi; a thin-layer chromatography identification method of fructus schisandrae comprises the steps that 10 microliters of a test sample solution, 10 microliters of a control medicinal material solution and 10 microliters of a negative reference substance solution are sucked separately and dropped on a same silica gel G thin layer plate to be unfolded, and the silica gel G thin layer plate is taken out, aired and inspected under an ultraviolet lamp; a thin-layer chromatography identification method of radix asparagi comprises the steps that 5 microliters of a test sample solution, 5 microliters of a control medicinal material solution and 5 microliters of a negative reference substance solution are sucked separately and dropped on a same silica gel G thin layer plate taking sodium carboxymethylcellulose as an adhesive to be unfolded, the silica gel G thin layer plate is taken out and aired, a 10% sulfuric acid ethanol solution is sprayed, and heating is conducted at 105 DEG C for color development. According to the method, fructus schisandrae and radix asparagi can be effectively identified, the quality standard of the variety is improved, and the important significance on production process quality controlling and product treatment effect guaranteeing is achieved.

Description

technical field [0001] The invention relates to a quality detection method of Changchun Yishou Gao, which belongs to the field of quality detection of traditional Chinese medicines. Background technique [0002] Changchun Yishou ointment, tonifies the five internal organs, regulates yin and yang, nourishes qi and blood, and strengthens muscles and bones. It is suitable for physical weakness and fatigue, premature aging and forgetfulness, palpitations, insomnia, weakness of the waist and knees, etc. The drug standard issued by the Ministry of Health (Traditional Chinese Medicine Prescription Volume 19) discloses its prescription and preparation method as follows: [0003] [Prescription] Asparagus 100g, Radix Ophiopogon 100g, Rehmannia glutinosa 100g [0004] Rehmannia glutinosa 100g Yam 100g Achyranthes bidentata 100g [0005] Eucommia leaves 100g Polygonum multiflorum 100g Ginseng 50g [0006] Poria Cocos 100g Woody Fragrance 100g Cypress Kernel 100g [0007] Schisandra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90
CPCG01N30/90
Inventor 耿秋霞
Owner JIANGSU 707 NATURAL PHARMA
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