Preparing method of gadus collagen protein peptide chelate
A technology of copper chelate and skin collagen, which is applied in the field of preparation of cod skin collagen peptide copper chelate, can solve the problems of rare peptide chelated copper ions, achieve good economic and social benefits, less environmental pollution, The effect of promoting development
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Embodiment 1
[0018] A preparation method of cod skin collagen peptide copper chelate, comprising the following steps:
[0019] (1) Weigh a certain amount of cod skin collagen peptide and copper sulfate, put them in a beaker, add 100ml of distilled water, fully mix and dissolve, and heat in a water bath;
[0020] (2) After fully reacting, add an appropriate amount of absolute ethanol, filter with suction, dry the filter residue under steam at 100°C, grind the product with a mortar, pass through a 60-mesh sieve, and weigh;
[0021] (3) Weigh 3.7224g of EDTA, dissolve it in hot water, dilute to 500ml, and place it for 24-48 hours for later use;
[0022] (4) Dissolve 0.2g PAN in ethanol, dilute to 100m with ethanol;
[0023] (5) Weigh 8g of cod skin collagen peptide powder and 2g of copper sulfate powder, fix the reaction temperature at 50°C, react for 30min, control the pH to 712, set each pH as a reaction control unit, after the reaction of each unit, in Absorbance was measured at the maxi...
Embodiment 2
[0027] A preparation method of cod skin collagen peptide copper chelate, comprising the following steps:
[0028] (1) Weigh a certain amount of cod skin collagen peptide and copper sulfate, put them in a beaker, add 100ml of distilled water, fully mix and dissolve, and heat in a water bath;
[0029] (2) After fully reacting, add an appropriate amount of absolute ethanol, filter with suction, dry the filter residue under steam at 100°C, grind the product with a mortar, pass through a 60-mesh sieve, and weigh;
[0030] (3) Weigh 3.7224g of EDTA, dissolve it in hot water, dilute to 500ml, and place it for 24-48 hours for later use;
[0031] (4) Dissolve 0.2g PAN in ethanol, dilute to 100m with ethanol;
[0032] (5) Weigh 8g of cod skin collagen peptide powder and 2g of copper sulfate powder, fix the reaction temperature at 50°C, react for 30min, control the pH to 712, set each pH as a reaction control unit, after the reaction of each unit, in Absorbance was measured at the maxi...
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