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A kind of production technology of ferro-titanium alloy powder

A production process and technology of ferrotitanium alloy, applied in the field of production process of ferrotitanium alloy powder, can solve the problems of substandard content of impurity elements, low metal yield and high price, and achieve high productivity, excellent performance and low energy consumption. Effect

Active Publication Date: 2019-10-25
CENT OF EXCELLENCE FOR ADVANCED MATERIALS +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The production of ferro-titanium mainly adopts the production process of reduction method, but due to the high oxygen content in the preparation process of the thermite method, the yield of metal produced is low, and the content of impurity elements is not up to the standard; the main raw material of the remelting method is titanium sponge, which is subject to The source is limited, the price is expensive, the production process needs to be vacuumed, and the cost is very high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A production process of ferro-titanium alloy powder, the specific steps are as follows: (a) crushing a reducing agent and a mixed ore containing ilmenite ore to a particle size of 5mm and 10mm respectively, and then crushing the crushed reducing agent and ilmenite-containing ore The mixed ore is mixed evenly to obtain a mixed material; the amount of the reducing agent added is 6% of the mass of the ilmenite-containing mixed ore; (b) the obtained mixed material is first heated to 500 ° C for 20 minutes, and then heated to 1200 ° C Roasting for 3h to obtain ilmenite sinter; (c) cooling the ilmenite sinter to room temperature and then grinding the ore, making the fineness less than 200 mesh after grinding and accounting for 75%; (d) utilizing microwave to heat the material after the grinding to 450°C, keep warm for 20 minutes; (e) cool the material after microwave heating to room temperature for two-stage grinding, the second-stage grinding fineness is less than 30 μm, acco...

Embodiment 2

[0020] A production process of titanium-iron alloy powder, the specific steps are as follows: (a) crushing the reducing agent and the mixed ore containing ilmenite ore to particle diameters of 3mm and 15mm respectively, and then crushing the crushed reducing agent and ilmenite-containing ore The mixed ore is mixed evenly to obtain a mixed material; the amount of the reducing agent added is 5% of the mass of the ilmenite-containing mixed ore; (b) the obtained mixed material is first heated to 600 ° C for 20 to 30 minutes, and then heated to Roasting at 1180°C for 4 hours to obtain ilmenite sintered ore; (c) cooling the ilmenite sintered ore to room temperature and then grinding the ore, making the fineness less than 200 mesh after grinding to account for 80%; (d) heating the ground sintered ore by microwave Heat the material to 400°C and keep it warm for 30 minutes; (e) cool the material after microwave heating to room temperature for two-stage grinding, and the fineness of the ...

Embodiment 3

[0022] A production process of ferro-titanium alloy powder, the specific steps are as follows: (a) crushing a reducing agent and a mixed ore containing ilmenite ore to a particle size of 5mm and 30mm respectively, and then crushing the crushed reducing agent and ilmenite-containing ore The mixed ore is mixed evenly to obtain a mixed material; the amount of the reducing agent added is 6% of the mass of the ilmenite-containing mixed ore; (b) the obtained mixed material is first heated to 550 ° C for 25 minutes, and then heated to 1150 ° C Roasting for 5h to obtain ilmenite sintered ore; (c) cooling the ilmenite sintered ore to room temperature and then grinding the ore, making the fineness less than 200 mesh after grinding and accounting for 75%; (d) utilizing microwave to heat the material after the grinding to 420°C, keep warm for 25 minutes; (e) Cool the material after microwave heating to room temperature for two-stage grinding, and the second-stage grinding fineness is less ...

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Abstract

The invention relates to a production process for ferro titanium powder. Features of ingredients of various titanium-containing iron ores are utilized, the proportion of the various titanium-containing iron ores is controlled and adjusted according to element contents of the various titanium-containing iron ores, ingredient complementation is carried out, comprehensive economic utilization of mixed ores is achieved, sintering conditions are optimized, carbonate in the ores is decomposed thoroughly, metal oxide is also reduced thoroughly, obtained ferro titanium sintered ores are excellent in property, energy consumption is small in a ferro titanium powder preparation process, the productivity is high, and the social benefit, the environmental benefit and the economic benefit are high.

Description

technical field [0001] The invention relates to the technical field of ferro-titanium alloy smelting, in particular to a production process of ferro-titanium alloy powder. Background technique [0002] Pure titanium is a silver-gray metal with metallic luster. It has good ductility when heated, and its powder is dark gray. As a strategic resource, titanium is mainly used in high-strength alloys for aircraft and missile structural components, high-temperature high-strength alloys such as gas turbine blades, age-hardening superalloys, high-temperature casting alloys, etc. Titanium forms two compounds with iron: TiFe 2 and TiFe, of which only TiFe is stable, and TiFe 2 Exists only in solid alloys. Ferro-titanium is an alloy of titanium and iron. The melting point of ferro-titanium is between 1400~1500℃ due to its different chemical composition, and its density is 5.7~6.4g / cm 3 . Ferro-titanium is widely used in metallurgical production. It can be used as a deoxidizer, deni...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22B34/12C22B1/02C22B5/10B22F9/20B22F9/04
CPCB22F9/04B22F9/20C22B1/02C22B5/10C22B34/1218
Inventor 张书彦温树文马艳玲高建波赵兰
Owner CENT OF EXCELLENCE FOR ADVANCED MATERIALS