Coated 3D (three dimensional) resin lens and preparation method thereof
A resin lens, 3D technology, used in glasses/goggles, optics, instruments, etc., can solve the problems of scratches on the surface and insufficient wear resistance.
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[0015] The invention provides a method for preparing a coated 3D resin lens, the preparation method comprising:
[0016] (1) mixing nano titanium particles with a surface modifier to obtain modified nano titanium particles;
[0017] (2) Mix the modified nano-titanium particles and the alcohol solvent according to the mass ratio of 1-3.5:100, and react at 20-50° C. for 15-20 min to obtain a solution containing titanium oxide nanoparticles;
[0018] (3) Mix the solution containing titanium oxide nanoparticles, ethylene glycol, tetrabutyl titanate, ethylenediamine and hardening solution, and react at 30-55°C for 10-20min to obtain a coating solution;
[0019] (4) Soak the resin lens in the coating solution and take it out, then perform the first baking and the second baking successively to obtain the coated 3D resin lens; wherein, the conditions for the first baking include: The temperature is 50-70° C., and the baking time is 10-15 minutes; the conditions for the second baking ...
Embodiment 1
[0031] Mix nano-titanium particles with octadecylamine at a mass ratio of 1:10 to obtain modified nano-titanium particles; mix modified nano-titanium particles with ethanol solvent at a mass ratio of 1:100 and react at 20°C 15min, obtain titanium oxide nanoparticle solution; 100g titanium oxide nanoparticle solution, 10g ethylene glycol, 15g tetrabutyl titanate, 5g ethylenediamine and 2g hardening solution VH-10 were ultrasonically mixed (the frequency of ultrasonic mixing 10kHz, ultrasonic mixing time is 5min), and react at 30°C for 10min to obtain the coating solution; soak the resin lens in the coating solution and take it out (the soaking time is 20min, and the soaking temperature is 30°C), and then Carry out the first baking and the second baking in sequence to obtain the coated 3D resin lens; wherein, the conditions of the first baking include: the baking temperature is 50°C, and the baking time is 10 minutes; the second baking The baking conditions include: the baking t...
Embodiment 2
[0033] Mix nano-titanium particles with hexadecylamine at a mass ratio of 1:15 to obtain modified nano-titanium particles; mix modified nano-titanium particles with ethylene glycol solvent at a mass ratio of 3.5:100, and heat at 50°C The reaction was carried out for 20 minutes to obtain a titanium oxide nanoparticle solution; 100 g of titanium oxide nanoparticle solution, 20 g of ethylene glycol, 25 g of tetrabutyl titanate, 8 g of ethylenediamine and 8 g of hardening solution VH-10 were ultrasonically mixed (ultrasonic mixing frequency of 20kHz, ultrasonic mixing time of 8min), and react at 55°C for 20min to obtain a coating solution; soak the resin lens in the coating solution and take it out (the soaking time is 30min, and the soaking temperature is 35°C) , followed by the first baking and the second baking to obtain the coated 3D resin lens; wherein, the conditions of the first baking include: the baking temperature is 70°C, and the baking time is 15 minutes; the second bak...
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