A method for quickly screening prohibited flavors and fragrances in cream
A technology of flavors and fragrances and cream, applied in the direction of material separation, analysis materials, instruments, etc., to achieve the effects of high detection sensitivity, fast analysis speed, high accuracy and precision
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[0023] The principles and advantages of the present invention will be explained and described below through specific embodiments, so that those skilled in the art can better understand the present invention. The following descriptions are only exemplary and do not limit the content thereof.
[0024] In a kind of method for quickly screening the illegal addition of flavor and fragrance in cream, the preparation of the sample solution to be tested comprises the following steps:
[0025] 1) Weigh 2.0g (accurate to 0.01g) of each cream sample into a 10mL sample tube.
[0026]2) Place the sample tube on the sample tray of the online automatic DSPE pretreatment device, which is a dual-arm control system loaded with vortex and centrifugal devices. The following process is automatically completed by the dual-arm system (MPS XL), add 10mL of 1% (v / v) acetic acid-acetonitrile / water (75:25, v / v) mixed solution, vortex and mix for 30s, then pipette 1mL of the upper layer solution In the...
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