Quality control method of radix cudramiae medicinal materials

A quality control method, the technology of piercing stones, applied in the field of quality control of piercing stones medicinal materials, can solve the problems of difficult to achieve the quality of medicinal materials, not strong pertinence, etc., and achieve good reproducibility and strong specificity

Pending Publication Date: 2020-05-08
GUIZHOU SHENGSHI LONGFANG PHARMA
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  • Abstract
  • Description
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  • Application Information

AI Technical Summary

Problems solved by technology

The existing technology only involves the inspection of the properties of piercing stone medicinal materials ("Quality Standards for Traditional Chinese Medicinal Materials and Ethnic Medicinal Materials in Guizhou Province"), and the pertinence is not strong. It is difficult to achieve the purpose of truly controlling the quality of medicinal materials by using these methods

Method used

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  • Quality control method of radix cudramiae medicinal materials
  • Quality control method of radix cudramiae medicinal materials
  • Quality control method of radix cudramiae medicinal materials

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Experimental program
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Embodiment

[0025] 1. Experimental instruments and medicinal materials

[0026] Herbs:

[0027] The piercing stone was provided by Guizhou Shengshi Longfang Pharmaceutical Co., Ltd. Place of Origin: (1) Guangdong (2) Guangxi (3) Liuzhou; and identified as the fresh or dried root of Maclura tricuspidata (Carr.) Bur. or Macluracochinchinensis (Lour.) Corner. Voucher specimens are deposited in Guizhou Shengshi Longfang Pharmaceutical Co., Ltd.

[0028] Instruments and reagents:

[0029] Electronic balance AUW-220D (Shimadzu, Japan); CNC ultrasonic cleaner KQ-500DE (Kunshan Ultrasonic Instrument Co., Ltd., Jiangsu Province); digital display constant temperature water bath HH-4 (Guohua Electric Co., Ltd.); constant temperature drying oven 101-1 type (Shanghai Puhong Instrument Factory), dryer; WFH-201B ultraviolet transmission reflectometer (Shanghai Jingke Industrial Co., Ltd.), Olympus MD-50 biological microscope and supporting imaging system, and routine Blades for microsectioning, glas...

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Abstract

The invention discloses a quality control method of a radix cudramiae medicinal material, and relates to the technical field of traditional Chinese medicinal materials. The method comprises the following steps: (1) microscopically identifying medicinal material powder; (2) determining the water content, total ash content and extract content ranges of the medicinal materials: the water content is not more than 13.0%, the total ash content is not more than 6.0%, the extract is determined by a hot dipping method under the condition of an alcohol-soluble extract determination method (the general rule 2201 of the four parts of the Chinese Pharmacopoeia 2015 edition), and dilute ethanol is used as a solvent and is not less than 10.0%; and (3) thin-layer chromatography identification; wherein inthe chromatogram of the test sample, fluorescent spots with the same color should be shown at the position corresponding to the chromatogram of the kaempferol reference substance. The scientific, complete, reliable and effective quality control method for the radix cudramiae medicinal material is established, and the method is high in specificity and good in reproducibility; meanwhile, the qualitystandard of the radix cudramiae medicinal material is established by adopting the method, and the internal quality and the medication quality of the medicinal material can be effectively evaluated and controlled.

Description

technical field [0001] The invention relates to the technical field of traditional Chinese medicinal materials, in particular to a quality control method for crushing stone medicinal materials. Background technique [0002] Punchstone is the fresh or dried root of Maclura tricuspidata (Carr.) Bur. or Macluracochinchinensis (Lour.) Corner. Can be excavated throughout the year, cut off branch roots, washed, used fresh or cut, sliced ​​and dried. According to the "Modern Dictionary of Chinese Materia Medica" records Chuanposhi, also known as Nuzhe "Supplement to Materia Medica", Zhegen "Preparation for Emergencies Qianjin Yaofang", Chuanposhi ("Preparation for Herbal Medicine"), Dimiangen, Laxa Niu Rushi ("Lingnan Vegetables and Medicine Records"), Chizhi (Hunan). It is the root of the moraceae plant Zheshu or thorn. The name Chuanposhi first appeared in "Lingnan Vegetable Medicine Record". "Supplements to Materia Medica" contains "Nu Zhe", which says: "It is born in the mo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N33/15G01N30/90G01N30/94G01N1/28G01N21/84G01N21/88
CPCG01N33/15G01N30/90G01N30/94G01N1/28G01N21/84G01N21/88G01N2021/8466
Inventor 张涛涛陈玉其何莉华
Owner GUIZHOU SHENGSHI LONGFANG PHARMA
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