Freezing drying method and drying device thereof
A technology of a drying device and a drying method, which is applied in the direction of drying solid materials, drying solid materials without heating, and promoting the preliminary treatment of solid material drying, which can solve problems such as insufficient freezing, incomplete drying, and short storage time, and achieve reduction Treatment cost, simple device structure, and sufficient freeze-drying effect
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Embodiment 1
[0029] A kind of freeze-drying method, comprises the following steps:
[0030] (1) Pretreatment: pick and wash Dendrobium officinale and drain, use the color-protecting solution to ultrasonically soak, take out and drain and wait to dry. The color-protecting solution is an aqueous solution of 0.5% sodium pyrophosphate, and the frequency of the ultrasound is 15kHz , the soaking time is 20min;
[0031] (2) manufacturing atmosphere: the dendrobium candidum in the step (1) is placed in the drying device, then the air in the drying device is all extracted, then feed nitrogen into the drying device to keep the nitrogen atmosphere inside;
[0032] (3) Low-pressure evaporation: make the air pressure inside the drying device half of the atmospheric pressure, and the oscillating temperature rise is that the atmospheric pressure rises by 10° every time the heat is kept for 20 minutes and then continues to rise until the internal air pressure of the drying device rises in a large number d...
Embodiment 2
[0035] A kind of freeze-drying method, comprises the following steps:
[0036] (1) Pretreatment: pick and wash Dendrobium officinale and drain, use the color-protecting solution to ultrasonically soak, take out and drain and wait to dry, the color-protecting solution is a 1% aqueous solution of sodium pyrophosphate, and the frequency of the ultrasound is 30kHz , the soaking time is 60min;
[0037] (2) manufacturing atmosphere: the dendrobium candidum in the step (1) is placed in the drying device, then the air in the drying device is all extracted, then feed nitrogen into the drying device to keep the nitrogen atmosphere inside;
[0038] (3) Low-pressure evaporation: Make the air pressure inside the drying device half of the atmospheric pressure, and the oscillating temperature rise is that the atmospheric pressure rises by 10° every time it is kept warm for 60 minutes and then continues to rise until the internal air pressure of the drying device rises greatly after a large n...
Embodiment 3
[0041] A kind of freeze-drying method, comprises the following steps:
[0042] (1) Pretreatment: pick and wash Dendrobium officinale and drain, use the color-protecting liquid to ultrasonically soak, take out and drain and wait to dry, the color-protecting liquid is an aqueous solution of 0.8% sodium pyrophosphate, and the frequency of the ultrasound is 20kHz , the soaking time is 30min;
[0043] (2) manufacturing atmosphere: the dendrobium candidum in the step (1) is placed in the drying device, then the air in the drying device is all extracted, then feed nitrogen into the drying device to keep the nitrogen atmosphere inside;
[0044] (3) Low-pressure evaporation: make the air pressure inside the drying device half of the atmospheric pressure, and the oscillating temperature rise is that the atmospheric pressure rises by 10° every time the heat is kept for 30 minutes and then continues to rise until the internal air pressure of the drying device rises in a large number durin...
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