Quick-drying durable luminescent material and preparation method thereof

A luminous material and durable technology, applied in the field of materials, can solve the problems of affecting normal use, short luminous time, and inability to dry quickly, etc., to achieve the effect of reducing the setting time and good quick-drying effect

Pending Publication Date: 2021-04-30
河北地质大学
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Chemiluminescence is excited by the energy of chemical reactions; electroluminescence is excited by voltage; photoluminescence is excited by electromagnetic radiation; triboluminescence is excited by mechanical energy; cathodoluminescence is excited by high-energy electron beams; X-ray luminescence is excited by Excited by X-rays, the existing luminescent materials do not emit light for a long time and cannot be quickly condensed after heating, which affects normal use

Method used

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Examples

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Comparison scheme
Effect test

preparation example Construction

[0020] A method for preparing a quick-drying and durable luminescent material, comprising the following steps:

[0021] Step 1: Mix 50 parts of deionized water, 12 parts of ethyl acrylate, 8 parts of methylcellulose, 3 parts of persulfuric acid, 1 part of aluminum sulfate, 2 parts of vinyltrimethoxysilane and 6 parts of propylene carbonate , and react at a temperature of 30-400° C. for 15-20 minutes under the protection of nitrogen to obtain a reaction solution A;

[0022] Step 2: take by weighing 55 parts of Sr 2 o 3 and 25 Al 2 o 3 Put 7-8 parts of nitric acid in the beaker and join in the beaker;

[0023] Step 3: Weigh 7 parts of Y 2 0 3 , 5 copies of Yb 2 0 3 and 1 Tm 2 0 3 added to the beaker;

[0024] Step 4: Place the beaker on a magnetic stirrer, stir well, and finally react to obtain a transparent solution. Pour the resulting solution into a plastic beaker, then add excess hydrofluoric acid to it, stir to make it evenly mixed, and then add Reaction solutio...

Embodiment 2

[0029] The invention provides a quick-drying and durable luminescent material. The composition of the luminescent material includes the following raw materials in parts by weight: 60 parts of deionized water, 14 parts of ethyl acrylate, 10 parts of methyl cellulose, 5 parts of persulfuric acid, 2 parts of aluminum sulfate, 3 parts of vinyltrimethoxysilane, 8 parts of propylene carbonate, Sr 2 o 3 57 copies, Al 2 o 3 27 copies, Y 2 0 3 8 copies, Yb 2 0 3 6 copies and Tm 2 0 3 2 copies;

[0030] A method for preparing a quick-drying and durable luminescent material, comprising the following steps:

[0031] Step 1: Mix 60 parts of deionized water, 14 parts of ethyl acrylate, 10 parts of methyl cellulose, 5 parts of persulfuric acid, 2 parts of aluminum sulfate, 3 parts of vinyltrimethoxysilane, and 8 parts of propylene carbonate , and react at a temperature of 30-400° C. for 15-20 minutes under the protection of nitrogen to obtain a reaction solution A;

[0032] Step 2...

Embodiment 3

[0039]The invention provides a quick-drying and durable luminescent material. The composition of the luminescent material includes the following raw materials in parts by weight: 70 parts of deionized water, 16 parts of ethyl acrylate, 12 parts of methyl cellulose, 6 parts of persulfuric acid, 4 parts of aluminum sulfate, 5 parts of vinyltrimethoxysilane and 10 parts of propylene carbonate, Sr 2 o 3 60 parts, Al 2 o 3 30 copies, Y 2 0 3 9 parts, Yb 2 0 3 7 copies and Tm 2 0 3 3 copies;

[0040] A method for preparing a quick-drying and durable luminescent material, comprising the following steps:

[0041] Step 1: Mix 70 parts of deionized water, 16 parts of ethyl acrylate, 12 parts of methyl cellulose, 6 parts of persulfuric acid, 4 parts of aluminum sulfate, 5 parts of vinyltrimethoxysilane and 10 parts of propylene carbonate , reacted at a temperature of 30-400°C for 15-20min under the protection of nitrogen to obtain a reaction solution

[0042] Step 2: take 60 p...

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PUM

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Abstract

The invention discloses a quick-drying durable luminescent material, which comprises the following raw materials in parts by weight: 50-70 parts of deionized water, 12-16 parts of ethyl acrylate, 8-12 parts of methyl cellulose, 3-6 parts of persulfuric acid, 1-4 parts of aluminum sulfate, 2-5 parts of vinyltrimethoxysilane, 6-10 parts of propylene carbonate, 55-60 parts of Sr2O3, 25-30 parts of Al2O3, 7-9 parts of Y203, 5-7 parts of Yb203, and 1-3 parts of Tm203. According to the luminescent material obtained by the method provided by the invention, under the same condition, the afterglow time is relatively long and can reach 600 minutes or above, and meanwhile, the drying time of the material is greatly reduced and can be shortened by 15 seconds or above, so that a very good quick-drying effect is achieved.

Description

technical field [0001] The invention relates to the field of materials, in particular to a quick-drying and durable luminescent material and a preparation method thereof. Background technique [0002] Substances that can emit light after being excited by the outside world are called luminescent materials, and luminescent materials are one of functional materials. People are no strangers to luminous substances, and they can be seen almost everywhere in the home or in public places. Luminescent substances are at the core of airport x-ray security inspection machines and computer monitors. Of course, they are not only used in expensive equipment, but also in banknotes that are commonly used. Luminescent substances have already become an indispensable material in people's daily life, and they are widely used in many aspects such as large-screen color display panels, lighting equipment, computer monitors, and fluorescence detection and immunoassay. Luminescent materials can be ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K11/78
CPCC09K11/7769
Inventor 曹秀玲岳沐慈寇小勇曹维存王俊锋翟志强
Owner 河北地质大学
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