Preparation method of nano-silver flexible conductive film
A silver flexible and conductive film technology, which is applied in the direction of equipment for manufacturing conductive/semiconductive layers, cable/conductor manufacturing, conductive layers on insulating carriers, etc., can solve the problem of easy falling off of nano silver wire layers, poor flexibility, and work Low efficiency and other problems, to achieve the effect of good chemical stability, excellent anti-corrosion performance, and stable electrical conductivity
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[0021] A preparation method of nano-silver flexible conductive film, the steps of which are:
[0022] S1 Preparation of flexible substrate layer: Melt the optical film particles required to form the substrate layer, and then use hot rollers to heat press at high temperature to form a film-like flexible substrate layer. The materials of the flexible substrate layer are PET, COP, COC , PI, PMMA or PC;
[0023] S2 coating preparation: Mix glycerin, water, polyvinyl alcohol pyrrolidone, silver nitrate, and chloride salt, then quickly heat up to 200-250°C, and keep stirring for 30-60 minutes to obtain the nano-silver wire stock solution;
[0024] S3 paint purification: Cool the obtained nano-silver wire stock solution to below 80°C, add water to dilute to obtain a nano-silver wire dilution solution, desalt and de-surfactant the diluted solution, and then concentrate to obtain a refined nano-silver wire solution, nanometer The treatment method of desalting and desurfactant of the s...
Embodiment 1
[0032] A preparation method of nano-silver flexible conductive film, the steps of which are:
[0033] S1 Preparation of flexible base material layer: melt the optical film particles required for forming the base material layer, and then use hot rollers to heat press at high temperature to form a film-like flexible base material layer, and the material of the flexible base material layer is PET;
[0034] S2 coating preparation: Mix glycerin, water, polyvinyl alcohol pyrrolidone, silver nitrate, and chloride salt, then quickly raise the temperature to 200°C, and continue stirring for 60 minutes to obtain the nano-silver wire stock solution;
[0035] S3 paint purification: Cool the obtained nano-silver wire stock solution to 75°C, add water to dilute to obtain a nano-silver wire diluent, desalt and remove surfactant from the diluent, and then concentrate to obtain a refined nano-silver wire solution, nano-silver The treatment method of desalting and desurfactant of line diluent i...
Embodiment 2
[0042] A preparation method of nano-silver flexible conductive film, the steps of which are:
[0043] S1 Preparation of flexible base material layer: Melt the optical film particles required for forming the base material layer, and then use a hot roller to heat press at high temperature to form a film-like flexible base material layer, and the material of the flexible base material layer is PMMA;
[0044] S2 coating preparation: Mix glycerin, water, polyvinyl alcohol pyrrolidone, silver nitrate, and chloride salt, then quickly raise the temperature to 250°C, and continue stirring for 30 minutes to obtain the nano-silver wire stock solution;
[0045] S3 paint purification: Cool the obtained nano-silver wire stock solution to below 60°C, add water to dilute to obtain a nano-silver wire dilution, desalt and de-surfactant the diluted liquid, and then concentrate to obtain a refined nano-silver wire solution, nano The treatment method of desalting and desurfactant of the silver lin...
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