Compound and liquid crystal composition and liquid crystal display device thereof
A compound and general formula technology, applied in the field of liquid crystal display devices, can solve the problems of narrow temperature range and insufficient contrast, and achieve the effects of wide temperature range, low threshold voltage and mild reaction
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[0235] The synthetic route of the compound of formula I-1-1-5 is as follows:
[0236]
[0237] Step 1. Preparation of compounds of formula 3
[0238] Add 20.2g of the compound of formula 1 ((4-ethoxy-2,3-difluorophenyl) boronic acid), 19.1g of the compound of formula 2 (2-bromo-6-fluorophenol) and 21.2g in a 500mL three-necked flask g sodium carbonate, fully dissolved with 290mL of a mixed solvent composed of toluene, ethanol and water (the volume ratio of toluene, ethanol and water is 15:7:7), under nitrogen protection conditions, add 0.07g dichlorodi-tert-butyl -(4-Dimethylaminophenyl)phosphine palladium(II), react at a temperature of 70°C to 80°C for 3h. After the reaction is complete, cool to room temperature, separate the liquids, extract the aqueous phase with toluene, combine the organic phases, wash the organic phases with water, dry them with anhydrous sodium sulfate, dissolve them in petroleum ether, pass through 10 g of 80-120 mesh silica gel, concentrate, and u...
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