Ecological electrode, electric energy storage device and preparation method thereof
A technology for storing electrical energy and electrodes, which is applied in electrode manufacturing, battery electrodes, non-aqueous electrolyte storage batteries, etc., can solve the problems of toxicity, flammability, and volatility, so as to improve mechanical stability, increase the stability range, and ensure electrochemical stability. The effect of stability
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[0113] The following are illustrative examples of the invention, relating to electrodes and batteries representing a device for storing electrical energy.
[0114] Preparation of electrodes
[0115] Using LiFePO 4 (P2 from Johnson Matthey) as active material. LiFePO 4 Also using Lepage et al. 46 Reported chemical oxidation of acetic acid and hydrogen peroxide to FePO 4 . Note that other active materials that are stable in the electrochemical stability window in contact with the aqueous electrolyte can also be used.
[0116] Electrodes for electrochemical evaluation in aqueous electrolytes were prepared by combining 84 wt% active material (LFP or FePO) previously dissolved in deionized water 4 ), 9 wt % carbon black Timcal C65 and 7 wt % sodium carboxymethyl cellulose (CMC from Sigma Aldrich 419273, Mw=90,000 g / mol) binder. The slurry was mixed for 20 minutes using a Kurabo Mazerustar KK-50S planetary agitator-deaerator to obtain a homogeneous slurry and spread on a 30 m...
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