Integrated full-angle excitation source for atomic fluorescence spectrometer

An atomic fluorescence, all-angle technology, applied in the field of analytical instruments, can solve problems such as the influence of instrument measurement sensitivity, achieve good measurement precision, improve measurement sensitivity, and compact structure.

Pending Publication Date: 2022-07-22
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since the entire circumference of the quartz tube atomizer can only receive excitation light within 180 degrees at most, the measurement sensitivity of the instrument will inevitably be affected

Method used

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  • Integrated full-angle excitation source for atomic fluorescence spectrometer
  • Integrated full-angle excitation source for atomic fluorescence spectrometer
  • Integrated full-angle excitation source for atomic fluorescence spectrometer

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] image 3It is a schematic diagram of the structure of the integrated full-angle excitation source of the present invention, which is composed of an excitation light source module and a ring atomizer module. The excitation light source module is a microwave coaxial resonant cavity, including an outer conductor 1, a microwave input port 2, a microwave antenna 3, an inner conductor 4, an outer gas inlet 5, a middle pipe 6, a middle gas inlet 7, an inner pipe 8, Inner layer gas inlet 9, standard sample tube 10, standard sample inlet 11; outer conductor 1, inner conductor 4, middle tube 6, inner tube 8, standard sample tube 10 are nested and coaxial in order from outside to inside, The inner conductor 4 , the middle tube 6 , the inner tube 8 and the sample tube 10 are flush at the outlet end face, and the inner conductor 4 , the middle tube 6 , the inner tube 8 and the standard sample tube 10 and the outer conductor 1 form a microwave in a nested coaxial structure. Resonant...

Embodiment 2

[0034] Figure 4 It is another structural schematic diagram of the integrated full-angle excitation source of the present invention, which is composed of an excitation light source module and a ring atomizer module. The excitation light source module is a microwave coaxial resonant cavity, which is the same as the excitation source in Embodiment 1, and will not be repeated here.

[0035] In this embodiment, the annular atomizer is arranged outside the outer conductor 1 of the microwave coaxial resonator above the microwave input port 2, and the guide ring 12 is located outside the outer conductor 1 above the microwave input port 2; the side surface of the guide ring 12 is designed There are a working gas inlet 13, a sample inlet 14 and a shielding gas inlet 15; the inner side of the guide ring 12 is sequentially installed with an inner layer guide pipe 16, a middle layer guide pipe 17 and an outer layer guide pipe 18, and the inner layer guide pipe 18. 16. The middle layer gu...

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Abstract

The invention discloses an integrated full-angle excitation source for an atomic fluorescence spectrometer, and belongs to the technical field of analytical instruments. The integrated full-angle excitation source is composed of an excitation light source module and an annular atomizer module. The excitation light source module comprises an outer conductor (1), a microwave input port (2), a microwave antenna (3), an inner conductor (4) and the like, and the annular atomizer module comprises a guide ring (12), a working gas inlet (13), a to-be-tested sample inlet (14) and the like. The excitation light source provided by the invention can be applied to an atomic fluorescence spectrometer, and has the advantages of high radiation intensity, narrow spectral line, good spectral selectivity, capability of exciting a detected sample at all angles in the 360-degree direction, and the like.

Description

technical field [0001] The invention belongs to the technical field of analytical instruments, in particular to an integrated full-angle excitation source for an atomic fluorescence spectrometer. Background technique [0002] In the atomic spectroscopic analysis instrument, the excitation source (atomicizer and / or excitation light source) is the key and core, which directly determines the structure and analysis performance of the instrument. In existing atomic fluorescence spectrometers, the excitation light source and the atomizer are physically separated. Usually, the atomizer uses a hydrogen-oxygen flame in a quartz tube furnace, and the excitation light source uses a high-intensity hollow cathode lamp. The quartz tube atomizer is only suitable for elements that can generate gaseous hydrides at room temperature. The hydrogen generated by the hydride generation method and the oxygen in the air are burned in an argon atmosphere to achieve sample atomization. Therefore, th...

Claims

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Application Information

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Patent Type & AuthorityApplications(China)
IPC IPC(8): G01N21/64
CPCG01N21/6428G01N2021/6432
Inventor曹彦波宋大千高德江费强马品一于永
OwnerJILIN UNIV