The present application relates to a kind of spent fuel
insoluble residue processing and
analysis method, comprising extracting residue,
drying and weighing, strengthening
dissolution, analyzing residue heavy
uranium plutonium content and the like steps;Among them, through blank filter membrane contrast and eluent double baseline control, the interference influence of the
filtration process in residue analysis is significantly reduced, so that
nuclear material weighing result is more quantitative and reliable, conservative and reliable.Through in
small sample amount,
high radiation, complex multiphase matrix condition, using optimized mixed acid
system proportioning and reaction time / temperature window, the full
dissolution of trace target
nuclide uranium /
plutonium is realized, the purpose of quantitative analysis of target
nuclide in high radioactivity residue is achieved, to ensure the accurate determination and safe and efficient
processing of target
nuclide in residue.The present application will soluble nuclide be transferred into
liquid phase as far as possible, the source item intensity and volume of high-level
solid residue are reduced to the greatest extent, the burden of final
radioactive waste disposal is reduced, and it is suitable for
insoluble residue component analysis in
nuclear fuel reprocessing
plant.