Nicotine transdermal delivery system
A delivery system, nicotine technology, applied in nervous system diseases, sheet-like delivery, medical preparations of non-active ingredients, etc., can solve problems such as poor adhesion of percutaneous absorption preparations, highly complicated preparation methods, and reduced cohesion
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Embodiment 1-5
[0096] Under a nitrogen atmosphere, polymerize 2-ethylhexyl acrylate (95 parts), acrylic acid (5 parts) at 60°C in a separable flask equipped with a reflux condenser, a stirrer, a thermometer and a dropping funnel and a nitrogen insertion tube , ethyl acetate (100 parts) and benzoyl peroxide (benzoyl peroxide) (0.2 part, BPO, manufactured by NOF Corporation, product name is Nyper BW) 15 hours, obtain binder solution (hereinafter referred to as binder Solution A). 49.93, 54.923, 59.916, 64.909, and 69.902 parts of the obtained binder solutions A were taken with respect to the binder solid content, and placed in reaction containers, respectively. Add respectively 50, 45, 40, 35 and 30 parts of isopropyl myristate relative to the solid content of the binder in each reaction vessel, and then add 0.07, 0.077, 0.084, 0.091 and 0.098 parts (0.14% of the binder) of Coronate HL (manufactured by Nippon Polyurethane Industry Co., Ltd.), and the mixture was thoroughly stirred. Each of t...
Embodiment 6-10
[0099] The nicotine transdermal delivery system of Examples 6-10 was obtained in the same manner as in Example 1, except that Coconad MT (manufactured by Kao Corporation, caprylic acid capric triglyceride) was used instead of isopropyl myristate, respectively Binder solution A at 49.93, 54.923, 59.916, 64.909, 69.902 parts relative to binder solids, and Coconad MT at 50, 45, 40, 35 and 30 parts relative to binder solids and 0.07 , 0.077, 0.084, 0.091 and 0.098 parts (0.14% binder) of Coronate HL (manufactured by Nippon Polyurethane Industry Co., Ltd.).
Embodiment 11-14
[0101] Get 79.68, 69.72, 59.76 and 49.80 parts of 2-ethylhexyl acrylate / vinyl acetate / 2-hydroxyethyl acrylate=78 / 16 / 6 (weight ratio, DURO-TAK2196, National Starch & Chemical Company), respectively placed in the reaction vessel. Add 20, 30, 40 and 50 parts of Coconad MT (manufactured by Kao Corporation, caprylic acid capric acid triglyceride) relative to the amount of binder solids in each reaction vessel, and the addition ratio is 0.32, 0.28, 0.24 and 0.20 parts (of 0.4% of the binder) of ALCH (manufactured by Kawaken Fine Chemicals Co., Ltd., ethylacetoacetate·aluminum diisopropoxide) as a binder, and the mixture was thoroughly stirred. Each of the resulting solutions was used to prepare crosslinked adhesive layers of Examples 11-14 described below.
[0102] The resulting solution was applied to the peel-treated surface of a polyester film release liner having a peel-treated surface on one side to a thickness of 80 μm after drying, and an adhesive layer was obtained after dr...
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Abstract
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