Catalyst for controlling exhaust gas emission and method for manufacturing the same
A waste gas emission and catalyst technology, applied in chemical instruments and methods, catalyst activation/preparation, physical/chemical process catalysts, etc., can solve the problems that transition metals do not show catalytic activity and do not realize the reduction of precious metals, etc.
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Embodiment 1
[0066] The first step involves Pt(0.3wt.%)-Co(5.0wt.%)-Ce(8.8wt.%)-Al 2 O 3 Preparation of powder. Using cerium acetate aqueous solution will have a specific surface area of 200m 2 / g of alumina was soaked and impregnated, dried at 120°C overnight, and calcined at 600°C for 3 hours to obtain powder. At this time, a powder supporting 8.8 wt.% Ce when converted to oxide was obtained. The powder is immersed and impregnated with a mixed aqueous solution of dinitrodiammine platinum and cobalt nitrate so that when converted to metal, it becomes 0.3 wt.% Pt and 5.0 wt.% Co. After that, it was dried overnight at 120°C, and calcined at 400°C for 1 hour, so as to obtain a catalyst powder.
[0067] The second step involves the coating of the honeycomb body. Place 50 grams of the catalyst powder obtained in the first step above, 5 grams of boehmite, and 157 grams of an aqueous solution containing 10% nitric acid in a ceramic pot (grinding pot) made of alumina and shake with alumina balls, A...
Embodiment 2
[0069] Using barium acetate instead of cerium acetate in Example 1, the same process as in Example 1 was performed to obtain alumina with a Ba loading amount of 7.8 wt.% when converted to oxide. Thereafter, the honeycomb body was coated in the same manner as in Example 1 to obtain a sample of Example 2.
Embodiment 3
[0071] Using praseodymium acetate instead of cerium acetate in Example 1, the same process as in Example 1 was performed to obtain alumina having a Pr loading amount of 8.8 wt.% when converted to oxide. After that, the honeycomb body was coated in the same manner as in Example 1 to obtain a sample of Example 3.
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