Bombax cotton phase-change material production method
A technology of phase change materials and manufacturing methods, applied in heat exchange materials, chemical instruments and methods, textiles and papermaking, etc., can solve the problems of adjusting the temperature range that cannot meet actual needs, the appearance of fabrics is sticky, and the practical value is poor. To achieve the effects of alleviating the change of ambient temperature, comfortable living environment and saving cooling and heating energy
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Embodiment 1
[0033] 50% PEG-1000, 25% 2D resin, 3% MgCl 2 ·6H 2 0 / citric acid mixture (molar ratio 15:1), 3% NaCl is formulated as a phase-change finishing agent, kapok / cotton (50 / 50) blended knitted fabrics are immersed in the finishing agent for two hours, and then untreated Extrude the excess finishing agent that forms cross-linking, pre-baking at 80°C for 7 minutes, baking at 140°C for 3 minutes, soaping at 60°C for 10 minutes with a bath ratio of 2g / L, and then rinsing with water Clean, dry at 100°C, and finally use the PyrisIDSC differential tracing calorimeter of the American Perkin-Elme company to detect the absorption and exothermic properties of the sample, that is, the DSC curve, see figure 1 .
Embodiment 2
[0035] 20% PEG-600, 15% 2D resin, 2% MgCl 2 ·6H 2 O / citric acid (molar ratio 12: 1), 9% NaCl is made into phase-change finishing agent, impregnated kapok blended fabric (48% kapok, 48% cotton, spandex 4%) for 1 hour, and then rolled with conventional finishing machinery Squeeze out the excess finishing agent that has not formed cross-linking with a stick, pre-bake at 40°C for 10 minutes, bake at 160°C for 1 minute, and soap at 60°C for 20 minutes with a bath ratio of 2g / L. Then rinse with clean water, dry at 100°C, and finally use the PyrisIDSC type differential tracing calorimeter from Perkin-Elme, USA to test the sample to obtain the DSC curve, see figure 2 .
Embodiment 3
[0037] 80% PEG-800, 20% 2D resin, 8% MgCl 2 ·6H 2 O / citric acid (molar ratio 10:1), 5% K 2 SO 1 Make phase change finishing agent, impregnate kapok fiber for 5 hours, squeeze out excess uncrosslinked finishing agent with equipment, pre-bake at 100°C for 3 minutes, bake at 80°C for 5 minutes, use 2g / L Soaping at 60°C for 20 minutes, then rinsing with clean water, drying at 100°C, and finally testing the DSC curve of the sample with the PyrisIDSC type differential tracing calorimeter of the American Perkin-Elme company, see image 3 .
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