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Micrometre level arachidonic acid emulsion and preparation thereof

A technology of arachidonic acid emulsion and arachidonic acid, which is applied in the field of micron-scale arachidonic acid emulsion and its preparation, can solve the problems of cumbersome use process, easy oxidation, and difficulty in mixing uniformly, so as to reduce production and application The cost, the production process is simple and feasible, and the effect of good dispersion performance

Active Publication Date: 2012-07-04
湖北福星生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

ARA oil is easily oxidized when exposed to air, and cannot withstand high temperature, so it is difficult to directly use it in infant formula under the condition of effectively maintaining its activity
If ARA oil is microencapsulated and then added to formula food, although it can effectively solve the defect of its easy oxidation and deactivation and maintain its activity in use, it also has the disadvantages of cumbersome addition and use process and difficulty in mixing uniformly. , and the energy consumption in the process of ARA oil microencapsulation is extremely high, which greatly increases the production cost

Method used

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  • Micrometre level arachidonic acid emulsion and preparation thereof
  • Micrometre level arachidonic acid emulsion and preparation thereof

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preparation example Construction

[0044] The preparation method of micron grade arachidonic acid emulsion, the steps are:

[0045] 1) Oil phase part: add arachidonic acid oil with a concentration higher than 40% into the oil phase emulsifier and antioxidant according to the above weight ratio, and heat the oil bath to 50-70°C to dissolve it to make an oil phase product A;

[0046] 2) Water phase part: Add water phase emulsifier, stabilizer and dispersant into water according to the above weight ratio, fully stir, heat to 60-90°C, keep for 20-60min, and make water phase product B;

[0047] 3) After the temperature of the water phase product B drops to 50-80°C, slowly add A to B, perform primary emulsification with a high-speed shearing machine, and obtain product C;

[0048] 4) pressure homogenize product C to obtain product D;

[0049] 5) The product D is sterilized and cooled to obtain the product E, which is an arachidonic acid emulsion.

[0050] In the preparation method of the emulsion, the sterilizatio...

Embodiment 1

[0055] Embodiment 1 The preparation method that contains ARA50g / kg emulsion:

[0056] Take by weighing 130 grams of mixed fats and oils with 40% arachidonic acid content, 0.1 gram of antioxidant (comprising natural vitamin E 0.04 gram, ascorbyl palmitate 0.06 gram), 10 grams of oil phase emulsifier (comprising 6 grams of lecithin, single 4 grams of glycerides), they are mixed while heating, and when the temperature rises to 65°C, they are immediately transferred to the water phase (water phase temperature is 75°C for 40 minutes, and then cooled to 65°C), and the water phase is emulsified 5 grams of agent (including 3 grams of sucrose fatty acid ester, 2 grams of Tween 60), 10 grams of dispersant (including 10 grams of maltose) and 60 grams of thickening and stabilizing agent (including 50 grams of gum arabic and 10 grams of xanthan gum), Supplement to a total amount of 1000 grams with deionized water. Slowly add, stir while adding, after complete addition, use a high-speed sh...

Embodiment 2

[0057] Embodiment 2 The preparation method that contains ARA50g / kg emulsion:

[0058] Take by weighing 130 grams of mixed fats and oils with 40% arachidonic acid content, 10.05 grams of antioxidants (comprising natural vitamin E4.05 grams, 6 grams of ascorbyl palmitate), 40 grams of oil phase emulsifiers (comprising 24 grams of lecithin, single 16 grams of glycerides), they are mixed while heating, and when the temperature rises to 65°C, they are immediately transferred to the water phase (the temperature of the water phase is 75°C for 40 minutes, and then cooled to 65°C), which contains an emulsifier of 22.5 gram (comprising 13.5 grams of sucrose fatty acid ester, 9 grams of Tween 60), 105 grams of dispersant (comprising 105 grams of maltose) and 180 grams of thickening and stabilizing agent (comprising 150 grams of gum arabic and 30 grams of xanthan gum). Ionized water was added to a total of 1000 grams. Slowly add, stir while adding, after complete addition, use a high-spe...

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Abstract

The invention discloses a micron-grade arachidonic acid emulsion liquid and a preparation method thereof. The emulsion liquid 1000g in total weight comprises 50g-150g of arachidonic acid, 10g-70g of oil-phase emulsifier, 0.1g-20g of antioxidant, 5g-40g of water-phase emulsifier, 60g-300g of thickened stabilizer, 10g-200g of dispersant and others of water. The emulsion liquid of the invention is O / W type, and the emulsion liquid with stable state and emulsified grain size of less than 1 micron is obtained mainly by the emulsifier and the thickened stabilizer of certain percentage go through the emulsification process with ARA oil and water. The task of the invention is to provide a formula for preparing an ARA emulsion liquid that can be dispersed in cold water and has good stability, and is stable against light, heat and oxygen, and the formula can be conveniently applied in the relevant industries of the drink industry, etc.

Description

technical field [0001] The invention relates to a micron-sized arachidonic acid emulsion and a preparation method thereof, in particular to the formulation, process and application of an arachidonic acid (ARA) emulsion that needs to be used in the food, medicine, health care products, and cosmetic industries . The product of the present invention is used as a nutrition fortifier. technical background [0002] Arachidonic acid is an omega-6 long-chain polyunsaturated fatty acid (PUFA) (5,8,11,14-eicosatetraenoic acid, C20:4). ARA is the most abundant C20PUFA in the human body. It mainly exists in organs, muscles and blood tissues. In addition to its main structural lipid role, it is also a number of bioactive substances derived from circulating eicosenoic acid. These active substances have Regulatory effects on lipoprotein metabolism, blood rheology, vascular elasticity, leukocyte function and platelet activation. However, ARA cannot be synthesized de novo in the human bod...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A23L1/30A23L33/12
Inventor 宁超美解秀娟李莹胡锐
Owner 湖北福星生物科技有限公司
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