Method for synthesizing quadrangle tungsten oxide nano-powder

A nano-powder and square technology, which is applied in the field of preparation of square tungsten oxide nano-powder, can solve the problems of single shape, difficulty in large-scale promotion, high energy consumption, etc., and achieve the effect of uniform size

Inactive Publication Date: 2009-04-15
XINJIANG UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] At present, the literature reports on tungsten oxide with special morphology can be roughly divided into three types: one is high-temperature synthesis, and the quality of the synthesized nanomaterials is also good, but it requires high equipment and

Method used

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  • Method for synthesizing quadrangle tungsten oxide nano-powder
  • Method for synthesizing quadrangle tungsten oxide nano-powder
  • Method for synthesizing quadrangle tungsten oxide nano-powder

Examples

Experimental program
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Effect test

Embodiment 1

[0022] Dissolve 0.5g of sodium tungstate and 0.2g of citric acid in 10ml of water respectively, adjust the pH value to 1 with 6mol / L HCl after mixing. After ultrasonic treatment for 10 minutes, the resulting turbid solution was added to a polytetrafluoroethylene reactor lined with stainless steel (filling degree 80%), and reacted at 120° C. for 12 hours; the resulting product was washed with deionized water and ethanol, respectively, and washed The finished powder was kept at 60°C for 60 minutes to obtain tungsten oxide nanopowder.

Embodiment 2

[0024] Dissolve 0.5g of sodium tungstate and 0.2g of citric acid in 10ml of water respectively, adjust the pH value to 1 with 6mol / L HCl after mixing. After ultrasonic treatment for 10 minutes, the resulting turbid solution was added to a microwave reactor lined with polytetrafluoroethylene (filling degree 80%), and reacted at 120° C. for 0.5 h; the obtained product was washed with deionized water and ethanol respectively, After washing, the powder was incubated at 60° C. for 60 minutes to obtain tungsten oxide nanopowder.

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Abstract

The invention relates to a preparation method of square tungsten oxide nano powder, belonging to the field of inorganic non-metallic materials. The content thereof is as follows: tungstenic acid deposition obtained by the reaction of sodium tungstate and hydrochloric acid is used as a precursor, citric acid is used as an auxiliary reagent, hydrochloric acid is used to adjust pH value and nano tungsten oxide is grown in a high-pressure autoclave by heating. Heating mode can be microwave heating and resistance wire heating, and the nanocrystalline grown is square. The characteristic of the square tungsten oxide powder material is that: the size of the square tungsten oxide is between 80 and 150nm. The advantages of the method are that: the process is simple, the cost is low and the shape and size of the tungsten oxide crystal are hydrothermally controlled by the citric acid auxiliary.

Description

Technical field: [0001] The invention relates to a preparation method of square tungsten oxide nanopowder, which belongs to the field of inorganic non-metallic materials. Background technique: [0002] Nano WO 3 It has a strong ability to absorb electromagnetic waves, can be used as an excellent absorbing material in the use of solar energy, and can be used as an important invisible material in the military; it also has a huge specific surface area and significant surface effects, and is a very promising application. catalyst for NO x 、H 2 S, O 3 , NH 3 Good sensitivity to various gases, and TiO 2 The performance of composite photocatalysts formed by such materials is better; it has been widely used in fuel cells, chemical sensors, photoelectric devices and other fields. In recent years, due to the development of tungsten oxide nanomaterials preparation technology, the discovery of metastable high-efficiency discoloration and proton transfer properties, based on the ul...

Claims

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Application Information

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IPC IPC(8): C01G41/02B82B3/00
Inventor 宿新泰王吉德孙庆军骆建敏解正峰黄艳党富民衡秋丽
Owner XINJIANG UNIVERSITY
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