Evaluation device of complex small crystal synthesis under magnetic field condition

Abstract

The invention relates to a device for evaluating synthesis of small crystals of complexes under the condition of a magnetic field, which belongs to the field of single-crystal growth. Introduction of a magnetic field interference mechanism into an experiment for synthesizing the small crystals of the complexes and evaluation and mastery of the influence rules of the magnetic field interference mechanism in due time have scientific significance on searching for crystal material seedlings with potential value. The invention provides an experimental facility which is suitable for the aim. The device comprises two flat boxlike objects which are overlaid together, and a plurality of cuplike objects, wherein walls of the cuplike objects are hollow walls; water inlet joints and water outlet joints are arranged on outer side faces of the cuplike objects; a water inlet joint and a water outlet joint of each cuplike object are communicated with the two flat boxlike objects respectively; and permanent magnets are arranged at the bottoms of the cuplike objects. The device is applied to observation and evaluation of related reaction and effects during the process of preparation of the small crystals of the complexes under the condition of magnetic field interference, and can guide and reinforce reaction tendency and crystallization orientation which accord with research targets of corresponding synthesis experiments.

Description

technical field [0001] The invention relates to a synthesis and evaluation device for small complex crystals under magnetic field conditions, and belongs to the field of C30B single crystal growth. Background technique [0002] The research work on the synthesis exploration, structural analysis and application evaluation of small complex crystals has dual significance. On the one hand, it is helpful to further explore the relevant scientific laws. Materials are also expected to be revealed in the process. [0003] The first thing to do in this type of research is to probe the synthesis conditions of new crystals, of which solvent evaporation at or near room temperature is usually given priority because of its mild manner. [0004] Because there are many conditions that may affect the growth rate and crystal quality of the small crystals of the complex, screening synthetic experiments are usually necessary. This type of screening experiments is generally carried out using ma...

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Problems solved by technology

[0006] During the time-consuming and labor-intensive exploration process described above, the most exciting thing is to accidentally discover seedlings of complex crystal materials with potential value in electricity, light, sound, and magnetism. However, the designer of this case noticed that the actual On the other hand, the chances of discovering potentially valuable complex crystal material seedlings are rare and rare, just like searching for needles in the deep sea

The reason is that the experimental methods adopted by general scientific research laboratories in the above-mentioned synthetic exploration process are too extensive, and there is no introduction to help cultivate seedlings of complex crystal materials with potential value in electricity, light, sound, magnetism, etc. Additional auxiliary guidance factors, which make the search for target crystals inefficient

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