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System for quantificationally collecting trace gas in rock group inclusion and use method thereof

A trace gas collection system technology, applied in the field of geochemical research, can solve problems such as polluting the environment, reducing vacuum, and affecting the transfer of trace gases

Active Publication Date: 2011-01-26
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During this repeated inhalation and exhaust process, under vacuum negative pressure, a small amount of mercury vapor will inevitably enter the gas collection chamber 205 together with the transferred gas, and under vacuum, the natural evaporation of mercury will also reduce the pressure in the vacuum chamber. The degree of vacuum will inevitably affect the transfer of trace gases, resulting in incomplete transfer of trace gases
At the same time, mercury is a poisonous and harmful substance, which not only endangers the physical and mental health of operators and analysts, but also pollutes the environment.
In addition, because the residual gas in the pipeline between the vacuum chamber 214 and the vacuum valve 218 cannot be collected, but the inner volume of the pipeline is much larger than the inner volume of the gold tube 219, it will also cause incomplete gas collection.

Method used

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  • System for quantificationally collecting trace gas in rock group inclusion and use method thereof
  • System for quantificationally collecting trace gas in rock group inclusion and use method thereof
  • System for quantificationally collecting trace gas in rock group inclusion and use method thereof

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Embodiment

[0040] The present invention will be further described below in conjunction with the accompanying drawings and embodiments.

[0041] In the figure, the present invention is composed of a sealed grinding unit, a trace gas collection and metering unit, a piston air pump (or a peristaltic pump), a water injection device and a vacuum unit, wherein the upper end of the grinding cylinder 401 and the lower end of the cylinder upper cover 405 Put the O-ring at the end of the cylinder, and then use the fastening bolt 406 to pass through the flange hole of the cylinder upper cover 405 to connect with the flange screw hole of the mill cylinder 401. The axis center of the cylinder upper cover 405 or about There are two combined valves in the symmetrical position, which are composed of valve stem, adjusting bolt, valve O-ring, valve stem O-ring, etc. One outlet of the combined valve can be fed with carrier gas (usually closed), and the other The outlet is respectively connected to one end ...

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Abstract

The invention discloses a system for quantificationally collecting trace gas in a rock group inclusion and a use method thereof, pertaining to the experimental field of geochemical investigation fieldThe invention discloses a system for quantificationally collecting trace gas in a rock group inclusion and a use method thereof, pertaining to the experimental field of geochemical investigation field not be taken for analysis in a closed container under a low negative pressure status, transfer collection is uncompleted, gas is inconvenient to be taken for analysis and sequent quantitative and qun not be taken for analysis in a closed container under a low negative pressure status, transfer collection is uncompleted, gas is inconvenient to be taken for analysis and sequent quantitative and qualitative analyses on a plurality of items can not be carried out simultaneously in the prior art.alitative analyses on a plurality of items can not be carried out simultaneously in the prior art.. The system consists of a rock sealing and milling unit, a trace gas transfer unit and a trace gas metering unit, wherein a gas storage metering tube 503 and a water storage tube 504 in the trace gas. The system consists of a rock sealing and milling unit, a trace gas transfer unit and a trace gas metering unit, wherein a gas storage metering tube 503 and a water storage tube 504 in the trace gas metering unit are made of glass and a gas extraction screw nut 502 is made of organic glass and other plastics; the gas storage metering tube 503 has small inside diameters, uniform upper and lower imetering unit are made of glass and a gas extraction screw nut 502 is made of organic glass and other plastics; the gas storage metering tube 503 has small inside diameters, uniform upper and lower inside diameters and the maximum internal volume of 500 microliters or 1,000 microliters, and the external of the gas storage metering tube is provided with scales (the measuring unit is microliter); tnside diameters and the maximum internal volume of 500 microliters or 1,000 microliters, and the external of the gas storage metering tube is provided with scales (the measuring unit is microliter); the center section of the water storage tube 504 takes the shape of a drum; and a sealing gasket 501 is a solid cylindrical plate made from silastic. The invention solves the problems that trace gas cahe center section of the water storage tube 504 takes the shape of a drum; and a sealing gasket 501 is a solid cylindrical plate made from silastic. The invention solves the problems that trace gas can

Description

technical field [0001] The invention relates to an experimental device in the field of geochemical research, in particular to an experimental device for transferring, quantitatively collecting and preserving trace gas in inclusions of rock groups by means of electromechanical sealing. Background technique [0002] In oil and gas exploration and development, using the geochemical characteristics of gas contained in rock group inclusions is an important means to further study the generation, preservation, migration and storage of oil and natural gas. Since the volume of the inclusion itself is quite small, the amount of gas contained is very small - it belongs to the category of trace amount, so how to accurately transfer, collect and quantitatively store the extremely small amount of gas released after the rock group inclusions are broken, for chromatography and mass spectrometry Qualitative and quantitative analysis of items such as , isotope, etc. has always been the techni...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N1/22
Inventor 饶丹郑伦举王强秦建中张美珍陈伟钧马亮帮蒋宏
Owner CHINA PETROLEUM & CHEM CORP