Quick-release medicinal composition and preparation method thereof
A technology of composition and medicine, which is applied in the fields of quick-release carrier and sedative-hypnotic drug composition and its preparation, can solve the problems of complex operation, high cost, long production cycle, etc., achieve rapid onset of effect, reduce gastrointestinal irritation, capture The effect of high bioavailability
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[0079] The present invention also provides a preparation method of the immediate-release pharmaceutical composition of the present invention, the steps are as follows: after indiplon and auxiliary materials are respectively passed through a 100-mesh sieve, the main drug, CCNa, PVPPXL, MCC , SiO 2 , lactose, vanillin, citric acid, and aspartame in an appropriate amount are mixed by equal addition method, and then magnesium stearate is added to mix evenly. The tablet weight is 200mg and the hardness is 30N-80N. Tablets, instant-release pharmaceutical compositions.
[0080] (2) Quality control
[0081] The present invention also provides a quality control method of the immediate-release pharmaceutical composition of the present invention, the steps are as follows:
[0082] Adopt high performance liquid chromatography (HPLC), UVD detector; Chromatographic column is C8 post; Mobile phase is acetonitrile-phosphate buffer saline (pH is 6.8) (38 / 62); Ultraviolet detection wavelength...
Embodiment 1
[0087] Indiplon 10mg
[0088] Croscarmellose Sodium 25mg
[0089] Crospovidone 40mg
[0090] Silica 3mg
[0092] Microcrystalline Cellulose 20mg
[0093] Lactose 90mg
[0094] Vanillin 1mg
[0095] Citric acid 8mg
[0096] Aspartame 1mg
[0097] After passing the main drug and auxiliary materials through a 100-mesh sieve, the main drug, CCNa, PVPP XL, MCC, SiO2, lactose, vanillin, citric acid, and aspartame were delivered in equal amounts according to the above-mentioned optimized ratio and content of the main drug. Add magnesium stearate and mix evenly, and prepare tablets with a tablet weight of 200 mg and a hardness of 30N to 80N by using the powder direct compression method.
Embodiment 2
[0099] Indiplon 5mg
[0100] Croscarmellose Sodium 30mg
[0101] Crospovidone 30mg
[0102]Silica 3mg
[0104] Pregelatinized starch 50mg
[0105] Lactose 71mg
[0106] Vanillin 2mg
[0107] Citric acid 6mg
[0108] Aspartame 2mg
[0109] The preparation method is the same as in Example 1.
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